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Chemical Structure| 41295-20-9 Chemical Structure| 41295-20-9

Structure of 41295-20-9

Chemical Structure| 41295-20-9

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Product Details of [ 41295-20-9 ]

CAS No. :41295-20-9
Formula : C13H13NO
M.W : 199.25
SMILES Code : CC1=CC=C(OC2=CC=C(N)C=C2)C=C1
MDL No. :MFCD00059858
Boiling Point : No data available
InChI Key :VPCGOYHSWIYEMO-UHFFFAOYSA-N
Pubchem ID :94519

Safety of [ 41295-20-9 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 41295-20-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 41295-20-9 ]

[ 41295-20-9 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 103058-87-3 ]
  • [ 41295-20-9 ]
  • [ 1020104-83-9 ]
YieldReaction ConditionsOperation in experiment
A solution of <strong>[103058-87-3]5-bromo-2-methoxy-pyridine-3-carbaldehyde</strong> (0.87 g, 4.03 mmol) in dry MeOH (15 mL) was treated with 4-p-tolyloxy-phenylamine (0.88 g, 4.43 mmol) and reflux for 2.5 h. The solution was cooled to 0 C. and treated slowly with NaBH4 (0.38 g, 10.1 mmol). The reaction stirred at room temperature overnight. Additional NaBH4 (0.38 g, 10.1 mmol) was added and the reaction was continued stirring for additional 6 h. The solvent was removed and the residue was partitioned between CH2Cl2 (20 mL) and water (10 mL). The organic portion was brought to the usual work-up to give a crude material. The product was yielded after chromatography purification (silica gel, 25% EtOAc/hexanes). MS (EI) 399, 401 (M+H)+.
  • 2
  • [ 33332-28-4 ]
  • [ 41295-20-9 ]
  • [ 1366234-46-9 ]
 

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