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Chemical Structure| 403842-84-2 Chemical Structure| 403842-84-2

Structure of 403842-84-2

Chemical Structure| 403842-84-2

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Product Details of [ 403842-84-2 ]

CAS No. :403842-84-2
Formula : C13H23F3N2O3S
M.W : 344.39
SMILES Code : CCCCCCCC[N+]1=CN(C)C=C1.O=S(C(F)(F)F)([O-])=O
MDL No. :MFCD06411717
InChI Key :BCVMAYRUJBXMAP-UHFFFAOYSA-M
Pubchem ID :16212746

Safety of [ 403842-84-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319
Precautionary Statements:P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313

Application In Synthesis of [ 403842-84-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 403842-84-2 ]

[ 403842-84-2 ] Synthesis Path-Downstream   1~8

  • 1
  • [ 2926-27-4 ]
  • [ 64697-40-1 ]
  • [ 403842-84-2 ]
  • 2
  • [ 616-47-7 ]
  • [ 111-83-1 ]
  • [ 2926-27-4 ]
  • [ 403842-84-2 ]
  • 3
  • [ 616-47-7 ]
  • [ 111-85-3 ]
  • [ 2926-27-4 ]
  • [ 403842-84-2 ]
  • 4
  • [ 2926-27-4 ]
  • 1-octyl-3-methyl-imidazolium bromide [ No CAS ]
  • [ 403842-84-2 ]
  • 5
  • [ 21252-69-7 ]
  • [ 333-27-7 ]
  • [ 403842-84-2 ]
  • 6
  • [ 1493-13-6 ]
  • [ 64697-40-1 ]
  • [ 403842-84-2 ]
  • 7
  • [ 33454-82-9 ]
  • 1-octyl-3-methyl-imidazolium bromide [ No CAS ]
  • [ 403842-84-2 ]
YieldReaction ConditionsOperation in experiment
In neat (no solvent); at 120℃; for 0.5h;Microwave irradiation; General procedure: a mixture of 1-methylimidazole (0.4105 g, 5 mmol), 1-bromobutane (0.6850 g, 5 mmol) was heated under microwave irradiation (or conventional heating) in a 10 mL pressurized glass tube fitted with a Teflon-coated septum at 80 C for 20 min. Then, LiOTf (0.78 g, 5 mmol) was added and the mixture was irradiated at 100 C for 20 min. After cooling, the mixture was diluted with MeCN (5 mL), and after removal of the precipitated salt LiBr, the filtrate was then filtered through Celite. The crude product was washed with Et2O and concentrated to give a colorless to pale yellow liquid (1.382 g, 96 % yield). The [BMIM]OTf was dried under reduced pressure. The purity and authenticity of the ionic liquids were confirmed by 1H and 13C NMR spectroscopy.
  • 8
  • [ 403842-84-2 ]
  • tetramethylammonium tetrakis-(3,5-bis(trifluoromethyl)phenyl)borate [ No CAS ]
  • 1-methyl-3-octyl-imidazolium tetrakis(3,5-bis-(trifluoromethyl)phenyl)borate [ No CAS ]
 

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