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Chemical Structure| 400620-76-0 Chemical Structure| 400620-76-0

Structure of 400620-76-0

Chemical Structure| 400620-76-0

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Product Details of [ 400620-76-0 ]

CAS No. :400620-76-0
Formula : C9H8BrNO4
M.W : 274.07
SMILES Code : CC(C1=CC=C(Br)C=C1[N+]([O-])=O)C(O)=O
MDL No. :MFCD26912246

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Application In Synthesis of [ 400620-76-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 400620-76-0 ]

[ 400620-76-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 400620-76-0 ]
  • [ 90725-50-1 ]
YieldReaction ConditionsOperation in experiment
93% With sulfuric acid; zinc; In ethanol; water; at 90℃; To a stirred solution of 2-(4-bromo-2-nitro-phenyl)propionic 0.800 g, 2.91 mmol) dissolved in 50% H2SO4 (6.2 mL)/EtOH (8.5 mL) was added Zn dust (0.76 g, 11.6 mmol) at 90 C. under nitrogen. The reaction was then treated in a manner analogous to the cyclization described above in example 6 to provide 0.61 g (93%) of 6-bromo-3-methyl-1,3-dihydro-indol-2-one. Analysis Theory: C, 47.82; H, 3.57; N, 6.20 Found: C, 47.80; H, 3.78; N, 5.83
 

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