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Chemical Structure| 38087-96-6 Chemical Structure| 38087-96-6

Structure of 38087-96-6

Chemical Structure| 38087-96-6

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Product Details of [ 38087-96-6 ]

CAS No. :38087-96-6
Formula : C14H12O3
M.W : 228.24
SMILES Code : O=C(C1=CC=CC=C1C2=CC=CC(OC)=C2)O
MDL No. :MFCD03426465

Safety of [ 38087-96-6 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis of [ 38087-96-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 38087-96-6 ]

[ 38087-96-6 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 92379-10-7 ]
  • [ 77-78-1 ]
  • [ 38087-96-6 ]
  • 2
  • [ 38087-96-6 ]
  • [ 92379-10-7 ]
YieldReaction ConditionsOperation in experiment
With boron tribromide; In dichloromethane; Step C: Preparation of 2-(3'-hydroxyphenyl)benzoic acid 2-(3-Methoxyphenyl)benzoic acid from Step B (6.53 g, 28.6 mmol) was dissolved in dry CH2Cl2 (100 mL) under argon and cooled to -78 C. Boron tribromide (62.9 mL of a 1.0 M solution in CH2Cl2, 62.9 mmol) was added dropwise and the solution was stirred overnight and allowed to warm slowly to ambient temperature. The resulting mixture was cooled in an ice bath and quenched carefully with water (200 mL), then extracted with CH2Cl2 (3*250 mL). The combined organic extracts were dried over Na2SO4, filtered, and concentrated under reduced pressure to give the titled product which was sufficiently pure for use in the next step.
 

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