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Chemical Structure| 3794-80-7 Chemical Structure| 3794-80-7

Structure of 3794-80-7

Chemical Structure| 3794-80-7

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Product Details of [ 3794-80-7 ]

CAS No. :3794-80-7
Formula : C6H11ClO2
M.W : 150.60
SMILES Code : O=C(Cl)OC(CC)(C)C
MDL No. :MFCD24141174

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Application In Synthesis of [ 3794-80-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 3794-80-7 ]

[ 3794-80-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 3794-80-7 ]
  • [ 56503-39-0 ]
  • ethyl 2-t-amyloxycarbonyloxyimino-2-cyanoacetate [ No CAS ]
YieldReaction ConditionsOperation in experiment
With triethylamine; In ether-toluene; benzene; EXAMPLE 17 A solution of t-amyl chloroformate (0.05 mol) in an ether-toluene mixture (30 ml) is cooled to -10C, and a solution of <strong>[56503-39-0]ethyl 2-hydroxyimino-2-cyanoacetate</strong> (7.2 g) and triethylamine (7.0 ml) in dry benzene (50 ml) is dropwise added thereto. The resulting mixture is allowed to stand at room temperature over night. The reaction mixture is admixed with water and filtered. The organic layer is separated, washed with water, dried and concentrated to give ethyl 2-t-amyloxycarbonyloxyimino-2-cyanoacetate (5.1 g) as an oil. IR absorption spectrum: 1810 cm-1 (CO of OCOO), 1740 cm-1 (CO of ester).
 

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