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Chemical Structure| 3720-84-1 Chemical Structure| 3720-84-1

Structure of 3720-84-1

Chemical Structure| 3720-84-1

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Product Details of [ 3720-84-1 ]

CAS No. :3720-84-1
Formula : C9H21Br2N
M.W : 303.08
SMILES Code : CC[N+](CC)(CCCBr)CC.[Br-]
MDL No. :MFCD00075131

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Application In Synthesis of [ 3720-84-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 3720-84-1 ]

[ 3720-84-1 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 295-64-7 ]
  • [ 3720-84-1 ]
  • 1-(3-triethylammonio)propyl-1,4,7,10,13-penta-azacyclopentadecane [ No CAS ]
  • 2
  • [ 295-64-7 ]
  • [ 3720-84-1 ]
  • [ 316147-15-6 ]
YieldReaction ConditionsOperation in experiment
10 mmol of (3-bromopropyl)triethylammonium bromide are added to 10 mmol of [15ane]-N5(*) dissolved in 50 ml of deionised water.. After heating at 90 C. for 12 hours under an inert atmosphere, the water is evaporated off.. The oily residue is washed twice with dichloromethane and then dissolved in 100 ml of ethanol.. Treatment with 4 ml of 10N HCl added dropwise, while cooling the balloon flask to 0 C., yields a flaky white precipitate which is filtered, washed with alcohol and then with ether and dried, yielding the expected product. Melting point: >200 C. (decomposition)
 

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