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Chemical Structure| 35387-93-0 Chemical Structure| 35387-93-0

Structure of 35387-93-0

Chemical Structure| 35387-93-0

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Product Details of [ 35387-93-0 ]

CAS No. :35387-93-0
Formula : C9H9IO3
M.W : 292.07
SMILES Code : COC(=O)C1=CC(I)=C(OC)C=C1
MDL No. :MFCD00052925
Boiling Point : No data available
InChI Key :GHNGBFHLUOJHKP-UHFFFAOYSA-N
Pubchem ID :316980

Safety of [ 35387-93-0 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 35387-93-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 35387-93-0 ]

[ 35387-93-0 ] Synthesis Path-Downstream   1~5

  • 1
  • [ 35387-93-0 ]
  • [ 20398-06-5 ]
  • [ 214360-78-8 ]
  • [ 23676-08-6 ]
  • methyl 6-methoxy-2',4',6'-trimethylbiphenyl-3-carboxylate [ No CAS ]
  • 3
  • [ 35387-93-0 ]
  • [ 25015-63-8 ]
  • [ 269410-10-8 ]
YieldReaction ConditionsOperation in experiment
[00381] In a reaction tube under nitrogen, a mixture of PdCl2(dppf)CH2Cl2 (21 mg; 0.026 mmol) and triethylamine (0.34 ml; 2.44 mmol) in dioxane (2.5 ml; dried over 4 A sieves) was sealed and stirred at 80 C. overnight (18 h). After cooling to room temperature, HB(pin) (0.19 ml; 1.31 mmol) was added followed by methyl 3-iodo-4-methoxybenzoate (251 mg; 0.859 mmol) in dioxane (2.5 ml; dried over 4 A sieves) the reaction mixture was stirred at 80 C. GC analysis after 18 hours showed the desired borate compound at 13.0 minutes.
  • 4
  • [ 269410-10-8 ]
  • [ 35387-93-0 ]
  • [ 4712-73-6 ]
  • 5
  • [ 35387-93-0 ]
  • [ 73183-34-3 ]
  • [ 269410-10-8 ]
 

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