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Chemical Structure| 34322-82-2 Chemical Structure| 34322-82-2

Structure of 34322-82-2

Chemical Structure| 34322-82-2

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Product Details of [ 34322-82-2 ]

CAS No. :34322-82-2
Formula : C5H13NO
M.W : 103.16
SMILES Code : COCCNCC
MDL No. :MFCD00144876
InChI Key :VGEMYWDUTPQWBN-UHFFFAOYSA-N
Pubchem ID :546877

Safety of [ 34322-82-2 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H225-H314
Precautionary Statements:P210-P233-P240-P241+P242+P243-P260-P264-P280-P301+P330+P331+P310-P303+P361+P353+P310+P363-P304+P340+P310-P305+P351+P338+P310-P370+P378-P403+P235-P405-P501
Class:8(3)
UN#:2734
Packing Group:

Application In Synthesis of [ 34322-82-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 34322-82-2 ]

[ 34322-82-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 34322-82-2 ]
  • [ 146137-78-2 ]
  • [ 945847-34-7 ]
YieldReaction ConditionsOperation in experiment
With potassium carbonate; In toluene; at 120℃; 2-Fluoro-5-trifluoromethyl-benzaldehyde (2.7g) and ethyl-(2- methoxy-ethyl) -amine (2.18g) are dissolved in toluene (20ml), and thereto is added potassium carbonate (5.83g) and the mxture is stirred at 120C overnight. The reaction solution is cooled to room temperature, and thereto are added ethyl acetate and a saturated brine and the mixture is separated, and the organic layer is washed with a saturated brine, and the mixture is dried over magnesium sulfate and concentrated under reduced pressure. The residue is purified by silica gel column chromatography (hexane : ethyl acetate = 19: 1→4: 1) to give 2-[ethyl-(2-methoxy-ethyl)- amino]-5-trifluoromethyl-benzaldehyde (3.75g). MS (m/z): 276 [M+H]+.
 

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