Home Cart Sign in  
Chemical Structure| 34207-44-8 Chemical Structure| 34207-44-8

Structure of 34207-44-8

Chemical Structure| 34207-44-8

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 34207-44-8 ]

CAS No. :34207-44-8
Formula : C7H6ClF3N2
M.W : 210.58
SMILES Code : NC1=CC(C(F)(F)F)=CC(N)=C1Cl
MDL No. :MFCD00466370
InChI Key :YCWXOQCYLKOSKL-UHFFFAOYSA-N
Pubchem ID :12402994

Safety of [ 34207-44-8 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319
Precautionary Statements:P264-P280-P302+P352-P305+P351+P338-P332+P313-P337+P313-P362

Application In Synthesis of [ 34207-44-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 34207-44-8 ]

[ 34207-44-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 34207-44-8 ]
  • [ 50594-82-6 ]
YieldReaction ConditionsOperation in experiment
With hydrogenchloride; sodium nitrite;copper(I) chloride; In dichloromethane; water; (b) Preparation of 3,4,5-trichlorobenzotrifluoride from 4-chloro-3,5-diaminobenzotrifluoride Concentrated hydrochloric acid (75 liters) was cooled to -20 C. and stirred while a solution of sodium nitrite (10.5 kg) in water (22.5 liters) and a solution of 4-chloro-3,5-diaminobenzotrifluoride (7.5 kg) in dichloromethane (22.5 liters) were both slowly added. The total time taken for addition was 6 hours. The temperature of the mixture was kept between -12 and -6. The mixture was stirred for a further 30 minutes at between -6 and -9, and then transferred slowly on to a mixture of cuprous chloride (7 kg) and concentrated hydrochloric acid (40 liters), kept at a temperature between 13 and 23 by water-cooling. The mixture was then stirred for about 90 minutes at 15. The dichloromethane layer was separated and the aqueous layer re-extracted with more dichloromethane (2*20 liters). The combined dichloromethane extracts were washed with water (3*30 liters) and then evaporated leaving an oil (6.06 kg). This was distilled (some material lost by spillage) at a pressure of 30 Torr to give the required 3,4,5-trichlorobenzotrifluoride (boiling range 84-92).
 

Historical Records

Technical Information

Categories

Related Functional Groups of
[ 34207-44-8 ]

Fluorinated Building Blocks

Chemical Structure| 1179444-82-6

A783607 [1179444-82-6]

2-Chloro-5-(trifluoromethyl)aniline hydrochloride

Similarity: 0.97

Chemical Structure| 39885-50-2

A672393 [39885-50-2]

2-Chloro-4-(trifluoromethyl)aniline

Similarity: 0.93

Chemical Structure| 1261567-27-4

A470025 [1261567-27-4]

2-Chloro-5-(difluoromethyl)aniline

Similarity: 0.92

Chemical Structure| 24279-39-8

A161901 [24279-39-8]

2,6-Dichloro-4-(trifluoromethyl)aniline

Similarity: 0.90

Aryls

Chemical Structure| 1179444-82-6

A783607 [1179444-82-6]

2-Chloro-5-(trifluoromethyl)aniline hydrochloride

Similarity: 0.97

Chemical Structure| 39885-50-2

A672393 [39885-50-2]

2-Chloro-4-(trifluoromethyl)aniline

Similarity: 0.93

Chemical Structure| 1261567-27-4

A470025 [1261567-27-4]

2-Chloro-5-(difluoromethyl)aniline

Similarity: 0.92

Chemical Structure| 24279-39-8

A161901 [24279-39-8]

2,6-Dichloro-4-(trifluoromethyl)aniline

Similarity: 0.90

Chemical Structure| 62476-58-8

A129500 [62476-58-8]

2-Chloro-3-(trifluoromethyl)aniline

Similarity: 0.88

Chlorides

Chemical Structure| 1179444-82-6

A783607 [1179444-82-6]

2-Chloro-5-(trifluoromethyl)aniline hydrochloride

Similarity: 0.97

Chemical Structure| 39885-50-2

A672393 [39885-50-2]

2-Chloro-4-(trifluoromethyl)aniline

Similarity: 0.93

Chemical Structure| 1261567-27-4

A470025 [1261567-27-4]

2-Chloro-5-(difluoromethyl)aniline

Similarity: 0.92

Chemical Structure| 24279-39-8

A161901 [24279-39-8]

2,6-Dichloro-4-(trifluoromethyl)aniline

Similarity: 0.90

Amines

Chemical Structure| 1179444-82-6

A783607 [1179444-82-6]

2-Chloro-5-(trifluoromethyl)aniline hydrochloride

Similarity: 0.97

Chemical Structure| 39885-50-2

A672393 [39885-50-2]

2-Chloro-4-(trifluoromethyl)aniline

Similarity: 0.93

Chemical Structure| 1261567-27-4

A470025 [1261567-27-4]

2-Chloro-5-(difluoromethyl)aniline

Similarity: 0.92

Chemical Structure| 24279-39-8

A161901 [24279-39-8]

2,6-Dichloro-4-(trifluoromethyl)aniline

Similarity: 0.90

Trifluoromethyls

Chemical Structure| 1179444-82-6

A783607 [1179444-82-6]

2-Chloro-5-(trifluoromethyl)aniline hydrochloride

Similarity: 0.97

Chemical Structure| 39885-50-2

A672393 [39885-50-2]

2-Chloro-4-(trifluoromethyl)aniline

Similarity: 0.93

Chemical Structure| 24279-39-8

A161901 [24279-39-8]

2,6-Dichloro-4-(trifluoromethyl)aniline

Similarity: 0.90