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Chemical Structure| 34034-87-2 Chemical Structure| 34034-87-2

Structure of 34034-87-2

Chemical Structure| 34034-87-2

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Product Details of [ 34034-87-2 ]

CAS No. :34034-87-2
Formula : C8H11ClO5
M.W : 222.62
SMILES Code : O=C(OCC)C(Cl)C(C(OCC)=O)=O
MDL No. :MFCD04114359
Boiling Point : No data available
InChI Key :JNQWFLVFHCCWPV-UHFFFAOYSA-N
Pubchem ID :10998635

Safety of [ 34034-87-2 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302+H312-H314
Precautionary Statements:P260-P264-P270-P280-P301+P312+P330-P301+P330+P331-P303+P361+P353-P304+P340+P310-P305+P351+P338+P310-P362+P364-P405-P501
Class:8
UN#:3265
Packing Group:

Application In Synthesis of [ 34034-87-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 34034-87-2 ]

[ 34034-87-2 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 6100-60-3 ]
  • [ 34034-87-2 ]
  • [ 855463-51-3 ]
  • 2
  • [ 34034-87-2 ]
  • [ 421-52-3 ]
  • C10H10F3NO4S [ No CAS ]
YieldReaction ConditionsOperation in experiment
43.06% In diethyl ether; at 90 - 95℃;Inert atmosphere; Commercially available trifluoroacetamide(39.9842g, 0.353717 mol) powderStir at room temperature with 400 mL THF in a 1000 mL 2-neck-round flask.Then phosphorous pentasulfide (31.4482 g, 0.141486 mol)Add powder and reflux Flow N2 gas while stirring. At this time to maintain 70 ~ 75 for reflux and stirred for 4 hours. After the reaction is finished,After evaporating the solvent with the rotary evaporator, remove the by-product white solid with THF and then distillation.Through yellow liquid form <strong>[421-52-3]trifluorothioamide</strong>(43.38 g, 95.0%) was obtained.
 

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Technical Information

• Acyl Group Substitution • Alkyl Halide Occurrence • Baeyer-Villiger Oxidation • Barbier Coupling Reaction • Baylis-Hillman Reaction • Bouveault-Blanc Reduction • Bucherer-Bergs Reaction • Catalytic Hydrogenation • Clemmensen Reduction • Complex Metal Hydride Reductions • Corey-Bakshi-Shibata (CBS) Reduction • Corey-Chaykovsky Reaction • Ester Cleavage • Fischer Indole Synthesis • General Reactivity • Grignard Reaction • Heat of Combustion • Henry Nitroaldol Reaction • Hiyama Cross-Coupling Reaction • Horner-Wadsworth-Emmons Reaction • Hydride Reductions • Kinetics of Alkyl Halides • Kumada Cross-Coupling Reaction • Lawesson's Reagent • Leuckart-Wallach Reaction • McMurry Coupling • Meerwein-Ponndorf-Verley Reduction • Passerini Reaction • Paternò-Büchi Reaction • Petasis Reaction • Peterson Olefination • Pictet-Spengler Tetrahydroisoquinoline Synthesis • Preparation of Aldehydes and Ketones • Preparation of Amines • Prins Reaction • Reactions of Aldehydes and Ketones • Reactions of Alkyl Halides with Reducing Metals • Reactions of Amines • Reactions with Organometallic Reagents • Reformatsky Reaction • Robinson Annulation • Schlosser Modification of the Wittig Reaction • Schmidt Reaction • Specialized Acylation Reagents-Carbodiimides and Related Reagents • Specialized Acylation Reagents-Ketenes • Stille Coupling • Stobbe Condensation • Substitution and Elimination Reactions of Alkyl Halides • Suzuki Coupling • Tebbe Olefination • Ugi Reaction • Wittig Reaction • Wolff-Kishner Reduction

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