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Chemical Structure| 34033-41-5 Chemical Structure| 34033-41-5

Structure of 34033-41-5

Chemical Structure| 34033-41-5

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Product Details of [ 34033-41-5 ]

CAS No. :34033-41-5
Formula : C6H4BrClN2O2
M.W : 251.47
SMILES Code : NC1=C([N+]([O-])=O)C=C(Br)C=C1Cl
MDL No. :MFCD03426655
InChI Key :IZJHDXGYFMAJQJ-UHFFFAOYSA-N
Pubchem ID :13443119

Safety of [ 34033-41-5 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H312-H315-H319-H332-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 34033-41-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 34033-41-5 ]

[ 34033-41-5 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 3460-23-9 ]
  • [ 34033-41-5 ]
  • 2
  • [ 34033-41-5 ]
  • [ 16429-44-0 ]
YieldReaction ConditionsOperation in experiment
With hydrogenchloride; iron; In methanol; at 8 - 16℃; for 16.0h; General procedure for the synthesis of U2To a stirred solution of Ui in MeOH (100 mL) were added concentrated HC1 (9 mL, 108 mmol, 1 2M) and iron powder (10.0 g, 179 mmol). The reaction mixture was stirred at 8-16C for 16 hours. After reaction was completed, the mixture was filtered. The filtrate was neutralized to pH 8 with NaHCO3 aqueous solution and filtered. The filtrate was extracted with EtOAc (100 mLx2). The combined extracts were washed with brine (200 mL), dried over anhydrous Na2SO4 and concentrated under reduced pressure to afford U2.
 

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