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Chemical Structure| 34010-15-6 Chemical Structure| 34010-15-6

Structure of 34010-15-6

Chemical Structure| 34010-15-6

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Product Details of [ 34010-15-6 ]

CAS No. :34010-15-6
Formula : C14H28O
M.W : 212.37
SMILES Code : CC/C=C\CCCCCCCCCCO
MDL No. :MFCD00009982
InChI Key :YGHAIPJLMYTNAI-ARJAWSKDSA-N
Pubchem ID :1712010

Safety of [ 34010-15-6 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 34010-15-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 34010-15-6 ]

[ 34010-15-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 2346-26-1 ]
  • [ 34010-15-6 ]
  • [ 913964-02-0 ]
YieldReaction ConditionsOperation in experiment
With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; toluene; at 20℃; for 5h; 2.1 3-[(11Z)-tetradec-11-en-1-yl]-1,3-<strong>[2346-26-1]oxazolidine-2,4-dione</strong> 420 mg (1.98 mmol) of (11Z)-tetradec-11-en-1-ol, in solution in 2 ml of tetrahydrofuran, are added to a solution of 200 mg (1.98 mmol) of 1,3-<strong>[2346-26-1]oxazolidine-2,4-dione</strong> and of 571 mg (2.18 mmol) of triphenylphosphine in 4 ml of tetrahydrofuran. 0.99 ml (2.2 mmol) of a 40% solution of diethyl azodicarboxylate in toluene is subsequently added dropwise. The mixture is stirred at ambient temperature for 5 h. The solvent is evaporated under reduced pressure and the evaporation residue is purified by chromatography on a column of silica gel, elution being carried out with a gradient of 10 to 50% of ethyl acetate in cyclohexane. 490 mg of a yellow oil are thus obtained. 1H NMR (CDCl3) delta (ppm): 5.25 (m, 2H), 4.60 (s, 2H), 3.45 (t, 2H), 2.10-1.80 (m, 4H), 1.65-1.45 (m, 2H), 1.40-1.05 (m, 14H), 0.90 (t, 3H).
 

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