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Chemical Structure| 33194-35-3 Chemical Structure| 33194-35-3

Structure of 33194-35-3

Chemical Structure| 33194-35-3
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Product Details of [ 33194-35-3 ]

CAS No. :33194-35-3
Formula : C4H10N2O
M.W : 102.14
SMILES Code : C[C@H](N)C(NC)=O
MDL No. :MFCD02094359

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Application In Synthesis of [ 33194-35-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 33194-35-3 ]

[ 33194-35-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 61275-22-7 ]
  • [ 33194-35-3 ]
YieldReaction ConditionsOperation in experiment
With sodium carbonate; In ethanol; at 60℃; for 0.0166667h; l-Alanine N-methylamide hydrochloride (0.58 g, 4.17 mmol) and sodium carbonate (0.56 g, 5.30 mmol) were stirred in ethanol (40 mL) at 60 C for 1 min, then cooled to room temperature, filtered and evaporated to yield the desired product; [alpha]D34 +2.0 (c 0.1, CH2Cl2); numax (NaCl disk)/cm-1 3364, 1646, 1575, 1456, 1413, 1375, 1318, 1272, 1160; deltaH (500 MHz, CDCl3) 7.29 (1H, br s, NH), 3.34 (1H, q, J 7.0, CH), 2.66 (3H, d, J 5.0, NCH3), 1.39 (2H, br s, NH2), 1.17 (3H, d, J 7.0, CHCH3); deltaC (125 MHz, CDCl3) 176.5 (C), 50.7 (CH), 25.7 (CH3), 21.6 (CH3); m/z (EI+): 102.1 (M+); HRMS (EI+): found M+, 102.0788. C4H10N2O1 requires, 102.0793.
 

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