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Chemical Structure| 328-73-4 Chemical Structure| 328-73-4

Structure of 328-73-4

Chemical Structure| 328-73-4

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Product Details of [ 328-73-4 ]

CAS No. :328-73-4
Formula : C8H3F6I
M.W : 340.00
SMILES Code : FC(F)(F)C1=CC(=CC(I)=C1)C(F)(F)F
MDL No. :MFCD00040837
InChI Key :VDPIZIZDKPFXLI-UHFFFAOYSA-N
Pubchem ID :630970

Safety of [ 328-73-4 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H227-H315-H319-H335
Precautionary Statements:P305+P351+P338

Application In Synthesis of [ 328-73-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 328-73-4 ]

[ 328-73-4 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 328-73-4 ]
  • [ 38136-70-8 ]
  • [ 1454306-38-7 ]
  • 2
  • [ 328-73-4 ]
  • [ 349-58-6 ]
YieldReaction ConditionsOperation in experiment
96% With water; ethylene glycol; potassium hydroxide; copper dichloride; In dimethyl sulfoxide; at 120℃; for 24h;Inert atmosphere; General procedure: To a test tube containing a magnetic bar was added aryl halide (1.0 mmol), CuCl2 (13.4 mg, 0.1 mmol), KOH (336 mg, 6.0 mmol), ethylene glycol(12 muL, 0.2 mmol), and DMSO/H2O (1.0 mL/0.5 mL). After flushing with argon, the mixture was stirred in a preheated oil bath at 120 °C for 24 h. After cooled to ambient temperature, the reaction mixture was distributed in aqueous HCl (5 percent) and ethyl acetate. The organic layer was washed with water and brine, dried over anhydrous MgSO4, and concentrated under vacuum. The crude product was further purified by column chromatography (EtOAc/n-Hexane) to provide the phenols.
  • 3
  • [ 328-73-4 ]
  • [ 100-47-0 ]
  • [ 21221-93-2 ]
  • 4
  • [ 1455-20-5 ]
  • [ 328-73-4 ]
  • [ 292638-85-8 ]
  • C20H18F6O2S [ No CAS ]
 

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