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Chemical Structure| 2987-53-3 Chemical Structure| 2987-53-3

Structure of 2987-53-3

Chemical Structure| 2987-53-3

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Product Details of [ 2987-53-3 ]

CAS No. :2987-53-3
Formula : C7H9NS
M.W : 139.22
SMILES Code : NC1=CC=CC=C1SC
MDL No. :MFCD00007708
InChI Key :WBRPQQSADOCKCH-UHFFFAOYSA-N
Pubchem ID :76337

Safety of [ 2987-53-3 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H301-H311-H315-H319-H331-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P310-P302+P352-P304+P340-P305+P351+P338-P311-P330-P361-P363-P403+P233-P405-P501
Class:6.1
UN#:2810
Packing Group:

Application In Synthesis of [ 2987-53-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 2987-53-3 ]

[ 2987-53-3 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 624-89-5 ]
  • [ 622-37-7 ]
  • [ 3463-02-3 ]
  • [ 13920-91-7 ]
  • [ 2987-53-3 ]
  • [ 104-96-1 ]
  • 2
  • [ 3177-20-6 ]
  • [ 2987-53-3 ]
  • [ 1609533-88-1 ]
YieldReaction ConditionsOperation in experiment
With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 70℃; for 1.5h; Step 1 [00140] To vial containing <strong>[3177-20-6]methyl 2,4-dichloropyrimidine-5-carboxylate</strong> (140 mg, 0.68 mmol) was added acetonitrile (1 mL), diisopropylethyl amine (0.24 mL, 1.4 mmol) and 2- (methylthio)aniline (94 mg, 0.68 mmol). The reaction was heated to 70 °C for 90 minutes and then cooled to room temperature and the solvent removed in vacuo. The residual solid was re-dissolved in dichloromethane (DCM) and then precipitated out via the addition of hexanes. The product was collected via filtration, rinsing with hexanes and used without further purification. Collected material (220 mg) was c. 50percent pure. LC retention time 1.08 min [J]. Mass Spectrometry ("MS") (E+) m/z: 310 (MH+).
  • 3
  • [ 54221-96-4 ]
  • [ 2987-53-3 ]
  • [ 1618679-78-9 ]
 

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