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Chemical Structure| 29604-75-9 Chemical Structure| 29604-75-9

Structure of 29604-75-9

Chemical Structure| 29604-75-9

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Product Details of [ 29604-75-9 ]

CAS No. :29604-75-9
Formula : C6H3Br2Cl
M.W : 270.35
SMILES Code : ClC1=CC=C(Br)C=C1Br
MDL No. :MFCD11845901
InChI Key :IJZDMPWKIBVVCQ-UHFFFAOYSA-N
Pubchem ID :14029662

Safety of [ 29604-75-9 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 29604-75-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 29604-75-9 ]

[ 29604-75-9 ] Synthesis Path-Downstream   1~8

  • 1
  • [ 615-57-6 ]
  • [ 29604-75-9 ]
  • 2
  • [ 29604-75-9 ]
  • [ 100130-11-8 ]
  • 3
  • [ 89379-50-0 ]
  • [ 29604-75-9 ]
  • 6
  • [ 29604-75-9 ]
  • 4-chloro-2,6-dinitro-<i>N</i>,<i>N'</i>-diphenyl-<i>m</i>-phenylenediamine [ No CAS ]
  • 7
  • [ 29604-75-9 ]
  • [ 98-80-6 ]
  • [ 860603-42-5 ]
YieldReaction ConditionsOperation in experiment
71% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In tetrahydrofuran; at 65.0℃; for 18.0h; General procedure: 2-iodophenol (2.2 g, 0.010 mol) Pd (PPh3) 4 (0.6 g, 0.010 mol) was added to Intermediate 1-1 (4.3 g, 0.012 mol)0.0005 mol) and potassium carbonate (2.8 g, 0.020 mol) in THF (100 mL), and the mixture was reacted at 65 C for 18 hours with stirring. After completion of the reaction, the reaction mixture was cooled, separated into H2O: MC and subjected to column purification (n-hexane: MC) to obtain 2.3 g (yield: 71%) Phenyl boronic acid (2.8 g, 0.024 mol) was added to <strong>[29604-75-9]2,4-dibromo-1-chlorobenzene</strong> (2.7 g, 0.010 mol)Mol) was added thereto, and the reaction mixture was synthesized in the same manner as in Example 1 (2) 1.9 g (yield: 71%). (M / z = 264)
  • 8
  • [ 29604-75-9 ]
  • [ 98-80-6 ]
  • C24H18FN [ No CAS ]
 

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[ 29604-75-9 ]

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