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Chemical Structure| 29418-67-5 Chemical Structure| 29418-67-5

Structure of 29418-67-5

Chemical Structure| 29418-67-5

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Product Details of [ 29418-67-5 ]

CAS No. :29418-67-5
Formula : C7H7BrN2O
M.W : 215.05
SMILES Code : O=C(NN)C1=CC=CC=C1Br
MDL No. :MFCD00051577
InChI Key :PQNLAYLOCZKPIY-UHFFFAOYSA-N
Pubchem ID :101460

Safety of [ 29418-67-5 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319
Precautionary Statements:P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313

Application In Synthesis of [ 29418-67-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 29418-67-5 ]

[ 29418-67-5 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 72287-26-4 ]
  • C23H24BClFNO3 [ No CAS ]
  • [ 29418-67-5 ]
  • 5-acetyl-3-chloro-9-fluoro-5,6-dihydro-8-[2-(1,3,4-oxadiazol-2-yl)phenyl]-dibenzo[b,f]azocine [ No CAS ]
YieldReaction ConditionsOperation in experiment
With sodium carbonate;tetrakis(triphenylphosphine) palladium(0); In ethanol; water; toluene; at 85℃; for 2h; To a solution of Example 246A (48 mg, 0.11 mmol) and Example 246B (25 mg, 0.11 mmol) in EtOH (1 mL) and toluene (1 mL) under an argon atmosphere were added 2M Na2CO3 (0.165 mL, 0.33 mmol) followed by Pd(PPh3)4 (13 mg, 0.011 mmol)). The resulting suspension was stirred under argon at 85° C. for 2 hours. The reaction was cooled to ambient temperature, concentrated and purified by preparative HPLC to give the title compound (8.8 mg). HPLC Rt=2.203 min. m/z=446.08.
  • 2
  • [ 29418-67-5 ]
  • [ 143982-40-5 ]
  • 2-bromo-N'-((imidazo[1,2-a]pyrimidin-2-yl)methylene)benzohydrazide [ No CAS ]
YieldReaction ConditionsOperation in experiment
72% In ethanol; for 5.0h;Reflux; General procedure: To a stirred solution of compound 3 (100 mg, 0.30 mmol) in ethanol was added corresponding benzohydrazides (1.0 mmol) and refluxed for 5 h. The reaction medium was poured into water and extracted with ethyl acetate. The organic layer was washed with water followed by brine solution, dried over anhydrous sodium sulphate, filtered and concentrated under reduced pressure, to obtain the pure compounds.
  • 3
  • [ 41042-12-0 ]
  • [ 29418-67-5 ]
  • (Z)-2-bromo-N'-(2-oxo-1-propylindolin-3-ylidene)benzohydrazide [ No CAS ]
 

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