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Chemical Structure| 2917-91-1 Chemical Structure| 2917-91-1

Structure of 2917-91-1

Chemical Structure| 2917-91-1

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Product Details of [ 2917-91-1 ]

CAS No. :2917-91-1
Formula : C7H15NO
M.W : 129.20
SMILES Code : CCN(CC)CC1OC1
MDL No. :MFCD00092652

Safety of [ 2917-91-1 ]

Application In Synthesis of [ 2917-91-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 2917-91-1 ]

[ 2917-91-1 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 2917-91-1 ]
  • [ 623-57-4 ]
  • [ 15285-59-3 ]
  • [ 3492-47-5 ]
  • [ 3069-29-2 ]
  • [ 850218-50-7 ]
  • [ 850218-51-8 ]
YieldReaction ConditionsOperation in experiment
at 60℃; for 6h; 309.00 parts of 3-(2-aminoethylamino)-propyldimethoxymethylsilane were mixed with 505.40 parts of freshly prepared organic phase from 1.1 with stirring and heated to 60° C. A slightly exothermic reaction took place. After about 2 hours, the exothermic reaction subsided, and the mixture was left to react further at 60° C. for 4 hours. It was then cooled to room temperature. Glycidyl groups could no longer be titrated. This was because alkylation of the primary amino group had taken place. 814.4 parts of a silane mixture (I) were thus obtained with the following main components:
  • 2
  • [ 109-89-7 ]
  • [ 106-89-8 ]
  • [ 2917-91-1 ]
  • [ 623-57-4 ]
  • [ 15285-59-3 ]
  • [ 3492-47-5 ]
YieldReaction ConditionsOperation in experiment
298.00 parts of diethylamine were combined with 12.25 parts of water. Then, with stirring, at 20° C., 377.60 parts of epichlorohydrin were added dropwise over the course of 10 hours. The mixture was then further stirred for a further 10 hours at 20° C., and then 506.7 parts of sodium hydroxide solution, aqueous, 30percent strength by weight, were added dropwise. After 3 hours (15-20° C.), the stirrer was switched off. An organic phase (501.5 parts) formed which was separated off. It consisted of about 384.0 parts glycidyldiethylamine, 60.0 parts N,N,N',N'-tetraethyl-1,3-diamino-2-hydroxypropane, 25.0 parts water, 24.5 parts N,N-diethyl-2-hydroxy-3-chloropropanamine, 1.0 part sodium chloride and 7.0 parts 3-dimethylamino-2-hydroxy-1-propanol.
  • 3
  • [ 2917-91-1 ]
  • [ 623-57-4 ]
  • [ 15285-59-3 ]
  • [ 3179-76-8 ]
  • [ 3492-47-5 ]
  • C20H47N3O4Si [ No CAS ]
  • C38H88N6O7Si2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
at 20 - 60℃; for 4h; 286.50 parts of 3-aminopropyldiethoxymethylsilane were mixed with 505.40 parts of the freshly prepared organic phase from 1.1 with stirring at room temperature and heated to 60° C. An exothermic reaction took place, during which the temperature was kept at 60° C. by cooling. As soon as the exothermic reaction had passed, the mixture was left to react further for 4 hours at 60° C. and only then cooled to room temperature. Glycidyl groups could no longer be titrated. This was because alkylation of the primary amino groups of the silane had taken place. This thus gave 791.9 parts of a silane mixture (II) with the following main components:
 

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