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Chemical Structure| 289-96-3 Chemical Structure| 289-96-3

Structure of 289-96-3

Chemical Structure| 289-96-3

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Product Details of [ 289-96-3 ]

CAS No. :289-96-3
Formula : C3H3N3
M.W : 81.08
SMILES Code : N1=NN=CC=C1
MDL No. :MFCD13193661
Boiling Point : No data available

Safety of [ 289-96-3 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 289-96-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 289-96-3 ]

[ 289-96-3 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 456-14-4 ]
  • [ 289-96-3 ]
  • [ 68049-17-2 ]
  • 2
  • [ 57297-29-7 ]
  • [ 289-96-3 ]
  • [ 58173-74-3 ]
  • 3
  • [ 289-96-3 ]
  • [ 221615-75-4 ]
  • 6'-methyl-3-[4-(methylsulfonyl)phenyl]-2,3'-bipyridine [ No CAS ]
YieldReaction ConditionsOperation in experiment
83% With potassium hydroxide; In acetonitrile; at 80℃; for 8h;Inert atmosphere; In a 10 mL vacuum tube, add 1,2,3-triazine 2a (8.1 mg, 0.10 mmol), 2- (4-methanesulfonylphenyl) -1- (6-methylpyridin-3-yl)- Ethanone 6b (29 mg, 0.1 mmol) and KOH (2.8 mg, 0.05 mmol). Nitrogen was replaced three times, then 0.5mL MeCN was added, and the reaction tube was placed at 80 C for 8h. The reaction was followed by TLC. After the reaction was terminated, CH2Cl2 (3x10mL) was added for extraction, the organic phase was separated, dried over Na2SO4, and the organic phase was concentrated in vacuo, and then subjected to column chromatography to obtain the target product 2d, yield (26.9mg, 83%) .
 

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