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Chemical Structure| 27038-46-6 Chemical Structure| 27038-46-6

Structure of 27038-46-6

Chemical Structure| 27038-46-6

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Product Details of [ 27038-46-6 ]

CAS No. :27038-46-6
Formula : C7H6BrNO2
M.W : 216.03
SMILES Code : O=C1C(C(CBr)=O)=CC=CN1
MDL No. :MFCD13173354

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Application In Synthesis of [ 27038-46-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 27038-46-6 ]

[ 27038-46-6 ] Synthesis Path-Downstream   1~2

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  • [ 27038-46-6 ]
  • [ 144186-57-2 ]
  • 2
  • [ 131674-40-3 ]
  • [ 27038-46-6 ]
YieldReaction ConditionsOperation in experiment
1 g With hydrogen bromide; bromine; acetic acid; at 60℃; for 4h; To a solution of l-(2-methoxypyridin-3-yl)ethanone (1 g, 6.62 mmol) in HBr/HOAc (30%, 20 mL) was added bromine (1.06 g, 6.62 mmol) at room temperature. The mixture was stirred at 60 C for 4 h. It was then cooled to room temperature and methyl tert-butyl ether (20 mL) was added to the mixture. A precipitate formed which was collected via vacuum filtration, collected and dried in vacuo to afford the title compound as a yellow solid. (1 g, 70 % yield).
 

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