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Chemical Structure| 2651-43-6 Chemical Structure| 2651-43-6

Structure of 2651-43-6

Chemical Structure| 2651-43-6

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Product Details of [ 2651-43-6 ]

CAS No. :2651-43-6
Formula : C3H7NO2
M.W : 89.09
SMILES Code : O=C(N)CCO
MDL No. :MFCD04039564
InChI Key :SMGLHFBQMBVRCP-UHFFFAOYSA-N
Pubchem ID :4145140

Safety of [ 2651-43-6 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 2651-43-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 2651-43-6 ]

[ 2651-43-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 2651-43-6 ]
  • [ 128-37-0 ]
  • [ 100-46-9 ]
  • [ 13304-62-6 ]
YieldReaction ConditionsOperation in experiment
With PPA; EXAMPLE 6 N-benzylacrylamide. 59 g of beta-hydroxypropionamide and 75 g of benzylamine were heated with 50 mg of 2,6-di-t-butyl-p-cresol for 7 hours in a temperature range of 120-170 C. until the evolution of ammonia was complete. After adding 2.2 g of polyphosphoric acid distillation was carried out in an oil pump vacuum; the subsequent redistillation with the addition of 1 ml of sulphuric acid yielded 92 g of N-benzylacrylamide, Bp0.1 113 C., which crystallized in the receiver. Mp (crude product): 53 C. NMR (CDCl3): delta=4.35 (d,2); 5.35-6.25 (m,3); 7.2 (s,5).
 

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