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Chemical Structure| 2642-32-2 Chemical Structure| 2642-32-2

Structure of 2642-32-2

Chemical Structure| 2642-32-2

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Product Details of [ 2642-32-2 ]

CAS No. :2642-32-2
Formula : C17H18N2O3
M.W : 298.34
SMILES Code : O=C(OCC1=CC=CC=C1)NCC(NCC2=CC=CC=C2)=O
MDL No. :MFCD00686953

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Application In Synthesis of [ 2642-32-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 2642-32-2 ]

[ 2642-32-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 2642-32-2 ]
  • [ 39796-52-6 ]
YieldReaction ConditionsOperation in experiment
96% With palladium 10% on activated carbon; hydrogen; In methanol; at 20℃; under 760.051 Torr; for 3h; General procedure: This procedure is illustrated for compound 11a. To a solution of compound 10a (170 mg, 0.77 mmol) in methanol (10 mL), 10% Pd/C was added. The reaction was hydrogenated at room temperature and atmospheric pressure for 3 h. Then the catalyst was filtered off through Celite, and the clear solution, taken to dryness, afforded the title compound as an oil. The reaction was monitored by TLC and, for stability problems, the amine was directly used in the subsequent reaction. Yield 97%.
 

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