Home Cart Sign in  
Chemical Structure| 262450-64-6 Chemical Structure| 262450-64-6

Structure of 262450-64-6

Chemical Structure| 262450-64-6

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 262450-64-6 ]

CAS No. :262450-64-6
Formula : C8H9BrO2
M.W : 217.06
SMILES Code : OCC1=CC(OC)=CC(Br)=C1
MDL No. :MFCD00229988
InChI Key :PPWBDINRNWYVFZ-UHFFFAOYSA-N
Pubchem ID :10608788

Safety of [ 262450-64-6 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H332-H335
Precautionary Statements:P261-P280-P305+P351+P338

Application In Synthesis of [ 262450-64-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 262450-64-6 ]

[ 262450-64-6 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 262450-64-6 ]
  • [ 262450-65-7 ]
  • 2
  • [ 262450-65-7 ]
  • [ 262450-64-6 ]
YieldReaction ConditionsOperation in experiment
With sodium tetrahydroborate; ethanol; In tetrahydrofuran; at 20℃; for 3h;Cooling with ice; NaBH4 (3.85 g; WAKO) was added to an ethanol (80 mL) and THF (20 mL) mixture solution of <strong>[262450-65-7]3-bromo-5-methoxybenzaldehyde</strong> (22 g) with ice cooling and the resulting mixture was stirred at room temperature for 3 hours. The resulting mixture was poured into ice water (300 mL) and ethyl acetate (300 mL) was added thereto to extract the mixture with and the organic layer was washed with saturated aqueous sodium bicarbonate solution (300 mL) and then dried. The solvent was evaporated under reduced pressure to give the title compound (22.05 g).(Intermediate 1 Rf (TLC)=0.6 (Hex:EtOAc=1:1))
 

Historical Records

Technical Information

Categories