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Chemical Structure| 253120-47-7 Chemical Structure| 253120-47-7

Structure of 253120-47-7

Chemical Structure| 253120-47-7

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Product Details of [ 253120-47-7 ]

CAS No. :253120-47-7
Formula : C9H9NO4
M.W : 195.17
SMILES Code : NC1=C(C(=O)OC)C=CC=C1C(=O)O
MDL No. :MFCD06200897
InChI Key :UXQCFHRNRAGKOY-UHFFFAOYSA-N
Pubchem ID :2794812

Safety of [ 253120-47-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 253120-47-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 253120-47-7 ]

[ 253120-47-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 253120-47-7 ]
  • [ 18107-18-1 ]
  • [ 57053-02-8 ]
YieldReaction ConditionsOperation in experiment
With methanol; In tetrahydrofuran; diethyl ether; at 20℃; Trimethylsilyldiazaomethane (9.12 mL, 18.24 mmol) (2M in diethyl ether) was added slowly to a solution of 2-amino-3-(methoxycarbonyl)benzoic acid (2.0 g, 10.25 mmol) in anhydrous 9 mL tetrahydrofuran and 6 mL methanol then the mixture was stirred overnight at room temperature. The reaction mixture was concentrated and purified by flashchromatography (1-6% methanol/CH2Cl2) to afford the title compound.
 

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