25309-39-1|Trimethyl pyridine-2,4,6-tricarboxylate| Ambeed

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Quality Control of [ 25309-39-1 ] Purity: 95% SDS Specification

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NMR

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Product Details of [ 25309-39-1 ]

CAS No. :	25309-39-1
Formula :	C₁₁H₁₁NO₆
M.W :	253.21
SMILES Code :	O=C(C1=NC(C(OC)=O)=CC(C(OC)=O)=C1)OC
MDL No. :	MFCD26792768
InChI Key :	RJRVGJDUSQEIGG-UHFFFAOYSA-N
Pubchem ID :	12560765

Safety of [ 25309-39-1 ]

GHS Pictogram:
Signal Word:	Warning
Hazard Statements:	H302-H315-H319-H335
Precautionary Statements:	P261-P305+P351+P338

Application In Synthesis of [ 25309-39-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 25309-39-1 ]

[ 25309-39-1 ] Synthesis Path-Downstream 1~22

1
[ 499-50-3 ]
[ 25309-39-1 ]
6-trichloromethyl-pyridine-2,4-dicarboxylic acid dimethyl ester [ No CAS ]

References: [1]Journal fur praktische Chemie (Leipzig 1954),1937,vol. <2> 147,p. 188,196.

2
[ 67-56-1 ]
[ 536-20-9 ]
[ 25309-39-1 ]

Yield	Reaction Conditions	Operation in experiment
95%	With sulfuric acid; for 6.0h;Reflux;	Trimethyl pyridine-2,4,6-tricarboxylate 2 was prepared usingreported method [44]. Pyridine tricarboxylic acid 1 (10 g, 47 mmol)in methanol (70 mL) with concentrated sulfuric acid, 98percent (5 mL)was heated under reflux for six hours until complete disappearanceof compound 1. The solution was neutralized with CaCO3,filtered and solvent was evaporated under reduced pressure. Thecrude product was recrystallised from toluene to give a whitecrystalline product; Yield: 95percent; m.p.: 161 C IR (mmax, KBr,cm1): 3462, 3304 (NH stretch), 2976, 1737 (CO), 1644 (CN),1488 (CAN); 1H NMR (DMSO-d6) dH: 8.54 (2H, apparent s), 3.95(9H, apparent s).

References: [1]Bioorganic Chemistry,2014,vol. 57,p. 148 - 154.
[2]Tetrahedron,1980,vol. 36,p. 123 - 129.
[3]Monatshefte fur Chemie,1917,vol. 38,p. 239.
[4]Helvetica Chimica Acta,2004,vol. 87,p. 156 - 166.

3
[ 25309-39-1 ]
[ 33454-82-9 ]
C₁₁H₁₁FNO₆⁽¹⁺⁾*2CF₃O₃S^(1-)*Li⁽¹⁺⁾ [ No CAS ]

References: [1]Bulletin of the Chemical Society of Japan,1991,vol. 64,p. 1081 - 1092.

4
[ 25309-39-1 ]
[ 66133-69-5 ]

References: [1]Tetrahedron,1980,vol. 36,p. 123 - 129.

5
[ 2026-48-4 ]
[ 25309-39-1 ]
[ 172041-77-9 ]

References: [1]Tetrahedron Asymmetry,1995,vol. 6,p. 2487 - 2494.

7
[ 929-59-9 ]
[ 25309-39-1 ]
methyl 2,13-dioxo-6,9-dioxa-3,12,18-triazabicyclo[12.3.1]octadeca-1⁽¹⁸⁾,14,16-triene-16-carboxylate [ No CAS ]

References: [1]Helvetica Chimica Acta,2004,vol. 87,p. 156 - 166.

8
[ 108-75-8 ]
permanganate (6 mol) [ No CAS ]
[ 25309-39-1 ]

References: [1]Helvetica Chimica Acta,2004,vol. 87,p. 156 - 166.

9
[ 25309-39-1 ]
2,6-Bis-((S)-4-isopropyl-4,5-dihydro-oxazol-2-yl)-isonicotinic acid methyl ester [ No CAS ]

References: [1]Tetrahedron Asymmetry,1995,vol. 6,p. 2487 - 2494.

10
[ 25309-39-1 ]
[ 172041-78-0 ]

References: [1]Tetrahedron Asymmetry,1995,vol. 6,p. 2487 - 2494.

11
[ 108-75-8 ]
<i>O</i>-<toluene-4-sulfonyl>-reserpic acid methyl ester [ No CAS ]
[ 25309-39-1 ]

References: [1]Tetrahedron,1980,vol. 36,p. 123 - 129.

12
[ 25309-39-1 ]
[ 74802-48-5 ]

References: [1]Tetrahedron,1980,vol. 36,p. 123 - 129.

13
[ 109-06-8 ]
[ 25309-39-1 ]

References: [1]Monatshefte fur Chemie,1917,vol. 38,p. 239.

14
[ 59656-71-2 ]
[ 25309-39-1 ]

References: [1]Monatshefte fur Chemie,1917,vol. 38,p. 239.

15
[ 25309-39-1 ]
N’-2,N’-4,N’-6-tris(4-hydroxybenzylidene)pyridine-2,4,6-tricarbohydrazide [ No CAS ]