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Chemical Structure| 25158-68-3 Chemical Structure| 25158-68-3

Structure of 25158-68-3

Chemical Structure| 25158-68-3

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Product Details of [ 25158-68-3 ]

CAS No. :25158-68-3
Formula : C8H5NO4
M.W : 179.13
SMILES Code : O=C1COC2=CC=C([N+]([O-])=O)C=C12
MDL No. :MFCD10696198

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Application In Synthesis of [ 25158-68-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 25158-68-3 ]

[ 25158-68-3 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 25158-68-3 ]
  • [ 33906-30-8 ]
  • 2-[<i>N</i>'-(5-nitro-benzofuran-3-ylidene)-hydrazino]-benzoic acid [ No CAS ]
  • 2
  • [ 25158-68-3 ]
  • [ 33906-30-8 ]
  • o-[(2,3-dihydro-5-nitrobenzofuran-3-ylidene)hydrazino]-benzoic acid [ No CAS ]
YieldReaction ConditionsOperation in experiment
0.800 g (86%) In pyridine; Step 1) Preparation of o-[(2,3-dihydro-5-nitrobenzofuran-3-ylidene)hydrazino]-benzoic acid 5-Nitro-3(2H)-benzofuranone (0.500 g, 2.79 mmol)[Tobias, P. et al. J. Amer. Chem. Soc., 1969, 91 (18), 5171-5173] and <strong>[33906-30-8]2-hydrazinobenzoic acid hydrochloride</strong> (0.526 g, 2.79 mmol) were combined in pyridine (10 mL) and stirred overnight at ambient temperature. The mixture was vacuum filtered and dried in vacuo to afford 0.800 g (86%) of title compound as a yellow solid: mp 210 C.(dec) which was used without purification.
 

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