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Chemical Structure| 24860-53-5 Chemical Structure| 24860-53-5

Structure of 24860-53-5

Chemical Structure| 24860-53-5

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Product Details of [ 24860-53-5 ]

CAS No. :24860-53-5
Formula : C16H12Cl2O2
M.W : 307.17
SMILES Code : ClCC(C1=CC=C(C2=CC=C(C(CCl)=O)C=C2)C=C1)=O

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Application In Synthesis of [ 24860-53-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 24860-53-5 ]

[ 24860-53-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 24860-53-5 ]
  • [ 69610-41-9 ]
  • [ 1007882-23-6 ]
YieldReaction ConditionsOperation in experiment
82% Add DSV101 (1.54g) to a 50ml three-necked flask,Potassium bromide (0.30 g), dimethyl sulfoxide (10 ml),After reacting at 75 C for 6 h, the temperature was lowered, and ammonium acetate (2.31 g) was added.L-Boc guanylaldehyde (1.99 g) was reacted at 40 C for 5 h. Add 100ml of water,The organic layer was washed with brine (100 ml)Separation by column chromatography2.56g solid DSV01,The yield is 82%.The purity is 95%
 

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