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Type HazMat fee for 500 gram (Estimated)
Excepted Quantity USD 0.00
Limited Quantity USD 15-60
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Chemical Structure| 24608-52-4 Chemical Structure| 24608-52-4

Structure of 24608-52-4

Chemical Structure| 24608-52-4

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Product Details of [ 24608-52-4 ]

CAS No. :24608-52-4
Formula : C5H9ClO2
M.W : 136.58
SMILES Code : O=C(Cl)OC(C)(C)C
MDL No. :MFCD17013431

Safety of [ 24608-52-4 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H225-H314-H331
Precautionary Statements:P210-P233-P280-P303+P361+P353-P304+P340+P310-P305+P351+P338
Class:6.1(3,8)
UN#:2742
Packing Group:

Application In Synthesis of [ 24608-52-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 24608-52-4 ]

[ 24608-52-4 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 24608-52-4 ]
  • [ 2978-58-7 ]
  • [ 113486-06-9 ]
  • 2
  • [ 20265-38-7 ]
  • [ 24608-52-4 ]
  • [ 161117-83-5 ]
YieldReaction ConditionsOperation in experiment
With triethylamine; In tetrahydrofuran; at 0 - 20℃;Inert atmosphere; Under a nitrogen atmosphere, 50.0 g of 2-methoxy-3-aminopyridine (I) (0.4 mol, 1.0 eq), 122.2 g of triethylamine (1.2 mol, 3.0 eq), and 250 mL of tetrahydrofuran were added to the reaction bottle in turn, and the solution was stirred clear.65.6g of tert-butyl chloroformate (0.48mol, 1.2eq) was added dropwise at a temperature of 0-10 C.After the addition is completed, the temperature is raised to room temperature and stirred overnight for reaction.Distill under reduced pressure to no fraction, add n-heptane, and wash twice with water.After distillation under reduced pressure to no fraction, tetrahydrofuran was added to obtain a tetrahydrofuran solution of compound (II).
 

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