Home Cart Sign in  
Chemical Structure| 24441-89-2 Chemical Structure| 24441-89-2

Structure of 24441-89-2

Chemical Structure| 24441-89-2

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 24441-89-2 ]

CAS No. :24441-89-2
Formula : C9H13ClN2
M.W : 184.67
SMILES Code : N=C(N)CCC1=CC=CC=C1.[H]Cl
MDL No. :MFCD00158720
InChI Key :WNSJACFIQOWCHL-UHFFFAOYSA-N
Pubchem ID :12621988

Safety of [ 24441-89-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 24441-89-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 24441-89-2 ]

[ 24441-89-2 ] Synthesis Path-Downstream   1~1

  • 1
  • sodium salt of 4-amino-5-nitroso-2-(2-phenylethyl)pyrimid-6-one [ No CAS ]
  • [ 56503-39-0 ]
  • [ 24441-89-2 ]
  • 4-amino-5-nitroso-2-(2-phenylethyl)pyrimid-6-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
With sodium methylate; sodium; In methanol; water; The sodium salt of 4-amino-5-nitroso-2-(2-phenylethyl)pyrimid-6-one, used as a starting material in the above preparation, was prepared as follows: 3-Phenylpropionamidine hydrochloride (4.33 g; prepared as described by P. W. Neber and A. Uber, Leibig's Annalen der Chemie, 1928, 467, 52) was added to a solution of sodium methoxide (prepared from 2.17 g. sodium and 37 ml. anhydrous methanol). Ethyl alpha-oximinocyanoacetate (3.34 g.) was added, and the mixture was refluxed with stirring for 5.25 hours and left to stand overnight. The mauve solid was filtered off and washed with a small quantity of anhydrous methanol to give the crude sodium salt of 4-amino-5-nitroso-2-(2-phenylethyl)pyrimid-6-one (3.9 g.). An aliquot was dissolved in water, and the solution was filtered and acidified to pH 4 with glacial acetic acid to give 4-amino-5-nitroso-2-(2-phenylethyl)pyrimid-6-one as a turquoise solid, m.p. 253 C. (with decomposition, sintering at 188 C.).
 

Historical Records

Technical Information

Categories