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Chemical Structure| 2402-96-2 Chemical Structure| 2402-96-2

Structure of 2402-96-2

Chemical Structure| 2402-96-2

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Product Details of [ 2402-96-2 ]

CAS No. :2402-96-2
Formula : C7H7NO2
M.W : 137.14
SMILES Code : CC(C1=CC=[N+]([O-])C=C1)=O
MDL No. :MFCD00955960
InChI Key :GUHDDRZAZNIQJB-UHFFFAOYSA-N
Pubchem ID :337542

Safety of [ 2402-96-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319
Precautionary Statements:P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313

Application In Synthesis of [ 2402-96-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 2402-96-2 ]

[ 2402-96-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 2402-96-2 ]
  • [ 7677-24-9 ]
  • [ 52689-18-6 ]
YieldReaction ConditionsOperation in experiment
38% With N,N-Dimethylcarbamoyl chloride; In dichloromethane; at 20℃; for 16.0h; [00461] To a solution of l-(pyridin-4-yl)ethanone N-oxide (0.5 g, 3.65 mmol) in DCM (8 mL) was added TMSCN (398 mg, 4.01 mmol). After stirring for 5 mins, dimethycarbamoyl chloride (431 mg, 4.01 mmol) was added and the reaction mixture was stirred at room temperature for 16 hrs. 10% of aq. K2CO3 (10 mL) was added, the aqueous layer was extracted with DCM (8 mLX3). The organic layer was dried over Na2SO4 and concentrated to give 4- acetylpicolinonitrile (200 mg, 38%). LC/MS: 147.1 (M+l)
 

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