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Chemical Structure| 23975-15-7 Chemical Structure| 23975-15-7

Structure of 23975-15-7

Chemical Structure| 23975-15-7

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Product Details of [ 23975-15-7 ]

CAS No. :23975-15-7
Formula : C10H6S2
M.W : 190.28
SMILES Code : C1(C#CC2=CC=CS2)=CC=CS1
MDL No. :N/A
InChI Key :UVIHBGIRBHGVTK-UHFFFAOYSA-N
Pubchem ID :637281

Safety of [ 23975-15-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H317-H319
Precautionary Statements:P280-P305+P351+P338

Application In Synthesis of [ 23975-15-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 23975-15-7 ]

[ 23975-15-7 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 704-38-1 ]
  • [ 23975-15-7 ]
  • 2
  • [ 23975-15-7 ]
  • [ 704-38-1 ]
YieldReaction ConditionsOperation in experiment
55% With oxygen; copper diacetate; potassium carbonate; aniline; In dimethyl sulfoxide; at 120℃;Schlenk technique; Sealed tube; General procedure: An oven-dried Schlenk tube was charged with a magnetic stir-bar, 1,2-diarylalkynes 1 (0.5mmol), aniline (0.6mmol), K2CO3 (0.5mmol), Cu(OAc)2 (0.075mmol), DMSO (3mL), The tube was sealed, and oxygen was purged through syringe. Reaction was stirred at 120C for 16-18h. After the reaction was finished, the reaction mixture was diluted in 30mL ethyl acetate, filtered on Celite pad. The organic portion was washed with a saturated solution of brine (8mL), saturated NH4Cl (8mL), a saturated solution of brine (8mL), dried (Na2SO4) and concentrated in vacuum, and the resulting residue was purified by silica gel column chromatography (hexane/ethyl acetate) to afford the desired products 2.
  • 3
  • [ 23975-15-7 ]
  • [ 244090-34-4 ]
  • 5,6-di(thiophen-2-yl)indolo[1,2-a]quinoline [ No CAS ]
 

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