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Chemical Structure| 2380-36-1 Chemical Structure| 2380-36-1

Structure of 2380-36-1

Chemical Structure| 2380-36-1

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Product Details of [ 2380-36-1 ]

CAS No. :2380-36-1
Formula : C14H23N
M.W : 205.34
SMILES Code : NC1=CC(C(C)(C)C)=CC(C(C)(C)C)=C1
MDL No. :MFCD00134096
InChI Key :MJKNHXCPGXUEDO-UHFFFAOYSA-N
Pubchem ID :75419

Safety of [ 2380-36-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302+H312+H332-H315-H319
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312+P330-P302+P352+P312-P304+P340+P312-P305+P351+P338-P332+P313-P337+P313-P362+P364-P501

Application In Synthesis of [ 2380-36-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 2380-36-1 ]

[ 2380-36-1 ] Synthesis Path-Downstream   1~5

  • 1
  • [ 2380-36-1 ]
  • [ 197223-39-5 ]
  • 2
  • [ 15181-11-0 ]
  • [ 2380-36-1 ]
  • 3
  • [ 26608-06-0 ]
  • [ 2380-36-1 ]
  • N-(dibenzofuran-3-yl)-N-(3,5-di-tert-butylphenyl)amine [ No CAS ]
YieldReaction ConditionsOperation in experiment
59% With tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate; In hexane; toluene; at 120℃; for 7h;Inert atmosphere; In a 200 mL three-necked flask, 4.2 g (17 mmol) of<strong>[26608-06-0]3-bromodibenzofuran</strong>, 5.2 g (25 mmol) of3,5-di-tert-butylaniline, 4.9 g(51 mmol) of sodium tert-butoxide.To this mixture were added 85 mL of toluene,A 10% hexane solution of tri (tert-butyl) phosphine0.3 mL was added, and the mixture was degassed by stirring under reduced pressure.To this mixture was added 98 mg (0.17 mmol) of bis (dibenzylideneacetone) palladium (0), and the mixture was heated and stirred at 120 C. for 7 hours under a nitrogen stream. After stirring, toluene was added to the mixture, which was suction filtered through Florisil, Celite, and alumina, and the filtrate was concentrated to obtain a solid. This solid was purified by silica gel column chromatography (developing solvent: toluene: hexane = 1: 3). The obtained solid was recrystallized from ethanol to obtain 3.7 g of a white solid in a yield of 59%. The synthesis scheme of Step 4 is shown below.
  • 4
  • [ 26608-06-0 ]
  • [ 2380-36-1 ]
  • C74H66N2O4 [ No CAS ]
  • 5
  • [ 99586-31-9 ]
  • [ 2380-36-1 ]
  • C40H37N3O2 [ No CAS ]
 

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