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Chemical Structure| 232944-38-6 Chemical Structure| 232944-38-6

Structure of 232944-38-6

Chemical Structure| 232944-38-6

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Product Details of [ 232944-38-6 ]

CAS No. :232944-38-6
Formula : C5H12O3S2
M.W : 184.28
SMILES Code : CS(=O)(OCCCSC)=O
MDL No. :N/A
InChI Key :JJRYDZAYWWFTQA-UHFFFAOYSA-N
Pubchem ID :22931856

Safety of [ 232944-38-6 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H312-H315-H319-H332-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 232944-38-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 232944-38-6 ]

[ 232944-38-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 232944-38-6 ]
  • [ 357913-53-2 ]
YieldReaction ConditionsOperation in experiment
Impure sulphide methanesulfonate (3.8 g) from step (A) was dissolved in chloroform (75 ml), and the solution added dropwise to 10% sulfuric acid (104 ml). During the addition, solid potassium permanganate (13.7 g) was also added in small portions. Upon completion of the additions, the reaction mixture was stirred at ambient temperature for 2 days. The reaction mixture was cooled with an ice/water bath and sodium bisulfite added in small portions until the reaction mixture was decolorized. The layers were separated and the aqueous layer was extracted with chloroform (three 100 ml aliquots). The combined organic layers were concentrated affording impure sulfone methanesulfonate (3.7 g).
 

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