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[ CAS No. 23128-74-7 ] {[proInfo.proName]}

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Chemical Structure| 23128-74-7
Chemical Structure| 23128-74-7
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Product Details of [ 23128-74-7 ]

CAS No. :23128-74-7 MDL No. :MFCD00134697
Formula : C40H64N2O4 Boiling Point : -
Linear Structure Formula :- InChI Key :OKOBUGCCXMIKDM-UHFFFAOYSA-N
M.W : 636.95 Pubchem ID :90004
Synonyms :

Safety of [ 23128-74-7 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P280-P305+P351+P338 UN#:N/A
Hazard Statements:H302 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 23128-74-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 23128-74-7 ]
  • Downstream synthetic route of [ 23128-74-7 ]

[ 23128-74-7 ] Synthesis Path-Upstream   1~3

  • 1
  • [ 20170-32-5 ]
  • [ 23128-74-7 ]
YieldReaction ConditionsOperation in experiment
68.2% With silica gel In 5,5-dimethyl-1,3-cyclohexadiene at 144℃; for 10 h; Inert atmosphere In a nitrogen atmosphere, 30 g of white solid A1 (0.108 mol),85 g of white solid B3 (0.226 mol) and 258 g of xylene were charged into the reaction equipment,Heat to reflux (144 ° C)The reaction-produced water and 15percent by weight of the organic solvent were separated from the reaction system,Into the water separator for water treatment; the same time, heating the reflux process,The reactor was in communication with a desiccator containing 60 g of silica gel (second dehydrator)The reaction system was dried using silica gel in a desiccator.then,The water-treated aqueous organic solvent was contacted with 100 g of silica gel (first dehydrating agent)The organic solvent obtained after the contact is returned to the reaction system; heated to reflux for 10h and then cooled,Filtered, washed twice with isopropanol,The filter cake was dried at 110 ° C for 4 h to give 58 g of a white solid product. The yield of the product is 68.2percent.
Reference: [1] Patent: CN104211616, 2016, B, . Location in patent: Paragraph 0087-0088
  • 2
  • [ 124-09-4 ]
  • [ 3062-64-4 ]
  • [ 23128-74-7 ]
Reference: [1] Russian Journal of General Chemistry, 2016, vol. 86, # 12, p. 2797 - 2803[2] Zh. Obshch. Khim., 2016,
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  • [ 6386-38-5 ]
  • [ 23128-74-7 ]
Reference: [1] Patent: CN104211616, 2016, B,
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