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Chemical Structure| 22635-62-7 Chemical Structure| 22635-62-7

Structure of 22635-62-7

Chemical Structure| 22635-62-7

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Product Details of [ 22635-62-7 ]

CAS No. :22635-62-7
Formula : C12H18O2
M.W : 194.27
SMILES Code : CC(OC12CC3CC(C2)CC(C3)C1)=O
Boiling Point : No data available
InChI Key :ZYLRDAOEBRPIGT-UHFFFAOYSA-N
Pubchem ID :519973

Safety of [ 22635-62-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319
Precautionary Statements:P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330

Application In Synthesis of [ 22635-62-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 22635-62-7 ]

[ 22635-62-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 15231-91-1 ]
  • [ 22635-62-7 ]
  • [ 128272-29-7 ]
YieldReaction ConditionsOperation in experiment
With sulfuric acid; In hexane; n-heptane; water; ethyl acetate; EXAMPLE 9 Preparation of 7-(1-adamantyl)-6-hydroxy-2-bromonaphthalene In a 100 ml flask, under a nitrogen atmosphere, are placed 2 g of 1-acetoxyadamantane and 20 ml of n-heptane, and 0.5 g of concentrated sulfuric acid is introduced drop by drop. At a temperature of about 22.C, 2.3 of 6-hydroxy-2-bromonaphthalene are added slowly and the mixture is left in vigorous agitation. The solvent is eliminated by filtration and the solid residue in suspension in the water is collected. The residue is filtered and then washed until neutrality is obtained. The resulting reddish solid is washed again with hexane until a colorless filtrate is obtained. After drying in a vacuum oven for 24 hours at 30 C one obtains a raw product which is chromatographed with a silica column using an ethyl acetate and hexane mixture of 1:9 as the eluent. After evaporation of the solvents, 1.3 g of desired raw product were obtained (Melting point: 218-224 C.).
 

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