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Chemical Structure| 219897-32-2 Chemical Structure| 219897-32-2

Structure of 219897-32-2

Chemical Structure| 219897-32-2

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Product Details of [ 219897-32-2 ]

CAS No. :219897-32-2
Formula : C17H16ClNO
M.W : 285.77
SMILES Code : OC1=CC=C2C=CC=CC2=C1C(N)C3=CC=CC=C3.[H]Cl
MDL No. :MFCD00068236
InChI Key :PRQUQNDKNZOGPF-UHFFFAOYSA-N
Pubchem ID :2747676

Safety of [ 219897-32-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis of [ 219897-32-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 219897-32-2 ]

[ 219897-32-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 3382-18-1 ]
  • [ 219897-32-2 ]
  • 9,10-dimethoxy-15-phenylnaphth[1,2-e][1,3]oxazino[2,3-a]isoquinoline [ No CAS ]
YieldReaction ConditionsOperation in experiment
82% With triethylamine; In 1,4-dioxane; at 100℃; for 1.5h;Microwave irradiation; General procedure: The mixture of the appropriate aminonaphtholhydrochloride (0.44mmol), 6,7-dimethoxy-3,4-dihydroisoquinoline (2a, 0.4mmol) or 3,4-dihydroisoquinoline (2b, 0.4mmol) and Et3N (60mg, 0.6mmol) in 1,4-dioxane (5mL) was placed in a 10mL reaction vial and heated in a CEM LabMate microwave reactor under the microwave conditions given depicted in Tables 1 and 2. The solvent was then evaporated off and the crude product was crystallized with cold EtOH (8-12mL), filtered off and recrystallized from EtOH (11-15mL).
 

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