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Chemical Structure| 214958-27-7 Chemical Structure| 214958-27-7

Structure of 214958-27-7

Chemical Structure| 214958-27-7

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Product Details of [ 214958-27-7 ]

CAS No. :214958-27-7
Formula : C13H9IN2
M.W : 320.13
SMILES Code : IC1=CC=C(C2=CN3C=CC=CC3=N2)C=C1
MDL No. :MFCD00452514

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Application In Synthesis of [ 214958-27-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 214958-27-7 ]

[ 214958-27-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 641144-16-3 ]
  • [ 214958-27-7 ]
  • 2-[4-(10-bromo-anthracen-9-yl)-phenyl]-imidazo[1,2-a]pyridine [ No CAS ]
YieldReaction ConditionsOperation in experiment
78% With sodium carbonate;tetrakis(triphenylphosphine) palladium(0); In 1,2-dimethoxyethane; water; for 7h;Heating / reflux; Ten point six grams (33 mmol) of 2-(4-iodophenyl)-imidazo [1,2-a] pyridine, 10 g (33 mmol) of <strong>[641144-16-3]10-bromoanthracene-9-boronic acid</strong> and 0.77 g of tetrakis (triphenylphosphine) palladium were dissolved into 100 milliliter of 1,2-dimethoxyethane, and adding 50 milliliter of 2.0M sodium carbonate aqueous solution, the resultant suspension was refluxed under heating for 7 hours. After completion of the reaction, separation with filtration was carried out and resultant crystals were washed with water and methanol, thereby obtaining 11.7 g of 2-[4-(10-bromo-anthracene-9-yl)-phenyl]-imidazo [1,2-a] pyridine (yield: 78 %).
 

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