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Chemical Structure| 210963-93-2 Chemical Structure| 210963-93-2

Structure of 210963-93-2

Chemical Structure| 210963-93-2

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Product Details of [ 210963-93-2 ]

CAS No. :210963-93-2
Formula : C9H11BrN2
M.W : 227.10
SMILES Code : BrC1=CN=C(N2CCCC2)C=C1
MDL No. :MFCD07781213

Safety of [ 210963-93-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 210963-93-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 210963-93-2 ]

[ 210963-93-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 121-43-7 ]
  • [ 210963-93-2 ]
  • [ 1150114-75-2 ]
YieldReaction ConditionsOperation in experiment
53% Add SM17 (10.00g, 44.03mmol) to a 250ml three-necked flask containing THF (tetrahydrofuran) (50ml), add n-butyllithium (1.44g, 22.42mmol) dropwise at -78 C, and keep it for 1h after the addition Trimethyl borate (3.33g, 32.03mmol) was added dropwise, the temperature was continued for 1h, and the temperature was raised to room temperature and stirred overnight. Hydrochloric acid (2mol / L) was added to adjust the pH to neutral, and then filtered to obtain a crude white product, which was slurried with n-heptane to obtain a white solid intermediate I-P-1 (4.45g, yield 53%).
 

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