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CAS No. : | 1980045-93-9 | MDL No. : | MFCD27996088 |
Formula : | C6H12ClNO | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | XUNIMIQTGGVJPR-UHFFFAOYSA-N |
M.W : | 149.62 | Pubchem ID : | 122360933 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P280-P301+P312-P302+P352-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
100% | With hydrogenchloride In 1,4-dioxane at 20℃; for 3h; | 104.1 Step 1. (3 -Aminobicvclor 1.1.1 Ipentan- 1 -yl ) ethanol. HC1 Dissolved /tvV-butyl (3 -(hydroxymethyl)bicyclo[ 1.1.1 Jpentan- 1 -yl)carbamate (500 mg, 2.344 mmol) in HC1 (4.0 M in dioxane) (17.6 ml, 70.3 mmol). The mixture was stirred at RT for about 3 h. The mixture was concentrated in vacuo to give the desired product as a solid in quantitative yield. LCMS m/z (M+H) calc’d: 114.08 ; found 114.18 |
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