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Chemical Structure| 197435-52-2 Chemical Structure| 197435-52-2

Structure of 197435-52-2

Chemical Structure| 197435-52-2

tert-Butyl (4-(pyridin-4-yl)phenyl)carbamate

CAS No.: 197435-52-2

4.5 *For Research Use Only !

Cat. No.: A1807482 Purity: 95%

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Product Details of [ 197435-52-2 ]

CAS No. :197435-52-2
Formula : C16H18N2O2
M.W : 270.33
SMILES Code : O=C(OC(C)(C)C)NC1=CC=C(C2=CC=NC=C2)C=C1

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Application In Synthesis of [ 197435-52-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 197435-52-2 ]

[ 197435-52-2 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 1692-15-5 ]
  • [ 131818-17-2 ]
  • [ 197435-52-2 ]
YieldReaction ConditionsOperation in experiment
75% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In 1,4-dioxane; water; at 90℃; for 14h; Suzuki coupling reaction of tert-butyl 4-bromophenylcarbamate (800 mg, 2.95 mmol) with 4-pyridineboronic acid (300 mg, 2.46 mmol) in the presence of Pd(PPh3)4 (57 mg, 0.05 mmol) and K2C03 (678 mg, 4.9 mmol) in dioxane- H20 (4: 1, 10 mL) at 90 C for 14 hr. tert-Butyl 4-(pyridin-4- yl)phenylcarbamate (600 mg, 75%) was obtained after flash column chromatography (DCM:MeOH, 20: 1).
  • 2
  • [ 131818-17-2 ]
  • [ 197435-52-2 ]
 

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