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Chemical Structure| 19733-55-2 Chemical Structure| 19733-55-2

Structure of 19733-55-2

Chemical Structure| 19733-55-2

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Product Details of [ 19733-55-2 ]

CAS No. :19733-55-2
Formula : C11H14N2O2
M.W : 206.24
SMILES Code : O=[N+](C1=CC=C(C2CNCCC2)C=C1)[O-]
MDL No. :MFCD14706176
InChI Key :IFEPNLVXIOKMEY-UHFFFAOYSA-N
Pubchem ID :17845800

Safety of [ 19733-55-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H312-H315-H319-H332-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 19733-55-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 19733-55-2 ]

[ 19733-55-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 19733-55-2 ]
  • [ 19733-56-3 ]
YieldReaction ConditionsOperation in experiment
With palladium on activated charcoal; hydrogen; In methanol; at 50 - 60℃; under 4500.45 - 6000.6 Torr; To a solution of 3-(4-nitrophenyl)piperidine (Compound 19) (1.0 g) in methanol (20-40 mL) in hydrogenator, 50% wet Pd/C (100-200 mg) was charged. The reaction mixture was heated to 50-60C under a hydrogen gas pressure of 6-8 kg/cm2 till the completion of reaction. After completion of reaction, reaction mixture was cooled to 25-30C, filtered it through celite bed and washed with methanol (5 mL). The filtrate was distilled under vacuum at 50C to afford the titled compound (Yield: 0.5 g; HPLC Purity: 76.10%).
 

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