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Chemical Structure| 19406-11-2 Chemical Structure| 19406-11-2

Structure of 19406-11-2

Chemical Structure| 19406-11-2

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Product Details of [ 19406-11-2 ]

CAS No. :19406-11-2
Formula : C9H13NO2
M.W : 167.21
SMILES Code : O=C(C1=C(C)N(C)C=C1)OCC
MDL No. :MFCD25960583
InChI Key :GDHXZQNQHWTMCM-UHFFFAOYSA-N
Pubchem ID :12211514

Safety of [ 19406-11-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 19406-11-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 19406-11-2 ]

[ 19406-11-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 19406-11-2 ]
  • [ 89776-57-8 ]
YieldReaction ConditionsOperation in experiment
With water; lithium hydroxide; In 1,4-dioxane; at 100.0℃; for 16h; Step B: 1,2-Dimethyl-JH-pyrrole-3-carboxylic acid To a solution of the product from Step A (5.3 g, 31.7 mmol) in 1 ,4-dioxane (60 mL) is added lM LiOH (2.66 g, 63.4 minol) in water (60 ml) and the reaction stirred at 100 C for cci 16 h. The reaction is allowed to cool to ambient temperature, diluted with water and acidified with 2M Rd. The resulting precipitate is collected by vacuum filtration to affordthe desired product. The filtrate is extracted with ethyl acetate and the organic extracts dried over magnesium sulphate, filtered and concentrated to obtain an additional crop of desired product.LC/1VLS (C7H9N02) no ionisation; RT 0.71 (Method B)
 

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