Home Cart Sign in  
Chemical Structure| 19212-27-2 Chemical Structure| 19212-27-2

Structure of 19212-27-2

Chemical Structure| 19212-27-2

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 19212-27-2 ]

CAS No. :19212-27-2
Formula : C10H9NO
M.W : 159.18
SMILES Code : N#CCC(CC1=CC=CC=C1)=O
MDL No. :MFCD07367088

Safety of [ 19212-27-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302+H312+H332-H315-H319-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312+P330-P302+P352+P312-P304+P340+P312-P305+P351+P338-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 19212-27-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 19212-27-2 ]

[ 19212-27-2 ] Synthesis Path-Upstream   1~2

  • 1
  • [ 19212-27-2 ]
  • [ 150712-24-6 ]
YieldReaction ConditionsOperation in experiment
60% With hydrazine In ethanol for 3 h; Heating / reflux A solution of 3-oxo-4-phenyl butyronitrile (Method 26; 0.58 g, 3.64 mmol) and hydrazine monohydrate (0.177 ml, 3.64 mmol) in EtOH(16ml) was heated to reflux for 3 hours. After cooling to25 C, the reaction was concentrated under reduced pressure, extracted with DCM (15 ml), and washed twice with brine. The organic layer was dried over anhydrousNa2S04 and concentrated to give an orange solid. The resulted solid was triturated with hexanes : ether (1: 1) solution and collected by filtration to afford the title compound as a yellow solid (0.38 g,60percent). 1H NMR (400 MHz, CDC13) 5 3.9 (s, 2 H), 4.89 (br s,1 H), 5.44 (s,1 H), 7.19-7. 34(m, 5H). MS: Calcd. : 173; Found: [M+H]+ 174.
References: [1] Patent: WO2005/49033, 2005, A1, . Location in patent: Page/Page column 99.
[2] Patent: WO2008/62026, 2008, A1, . Location in patent: Page/Page column 20.
  • 2
  • [ 19212-27-2 ]
  • [ 101-97-3 ]
  • [ 150712-24-6 ]
References: [1] Patent: US6559173, 2003, B1, .
 

Historical Records

Technical Information

Categories