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Chemical Structure| 19090-04-1 Chemical Structure| 19090-04-1
Chemical Structure| 19090-04-1
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Product Details of [ 19090-04-1 ]

CAS No. :19090-04-1
Formula : C9H8O2
M.W : 148.16
SMILES Code : O=C1COC2=CC=CC=C2C1
MDL No. :MFCD09996937
InChI Key :SHHLMGCHMMCOOS-UHFFFAOYSA-N
Pubchem ID :11137321

Safety of [ 19090-04-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 19090-04-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 19090-04-1 ]

[ 19090-04-1 ] Synthesis Path-Downstream   1~28

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  • chroman-3-one thiosemicarbazone [ No CAS ]
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YieldReaction ConditionsOperation in experiment
84% With benzophenone; at 210℃; for 0.5h;Inert atmosphere; The mixture of 2a (44 mg, 0.2 mmol) and Ph2O (400 mg) was heated to 210 °C under argon for 30 min. After cooling to the room temperature, the residue was purified on silica gel (PE/EtOAc, 30:1) to get the product as a colorless oil (25 mg, 84percent). 1H NMR (400 MHz, CDCl3): delta 7.26?7.22 (m, 1H), 7.14?7.12 (m, 1H), 7.06 (d, J=7.6 Hz, 2H), 4.41 (s, 2H), 3.62 (s, 2H); 13C NMR (100 MHz, CDCl3): delta 207.74, 154.65, 129.08, 128.58, 123.45, 121.63, 117.80, 73.08, 41.03 ppm. The date of the compound is identical with the described date of the reference.16
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