Home Cart Sign in  
Chemical Structure| 187975-62-8 Chemical Structure| 187975-62-8

Structure of 187975-62-8

Chemical Structure| 187975-62-8

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 187975-62-8 ]

CAS No. :187975-62-8
Formula : C10H13N3O2
M.W : 207.23
SMILES Code : O=C1OC[C@H](CC2=CC=C(NN)C=C2)N1
MDL No. :MFCD08458733

Safety of [ 187975-62-8 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 187975-62-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 187975-62-8 ]

[ 187975-62-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1116-77-4 ]
  • [ 187975-62-8 ]
  • [ 139264-17-8 ]
YieldReaction ConditionsOperation in experiment
at 90 - 98℃; for 2.5h;Heating / reflux;Product distribution / selectivity; The diluted reaction mixture containing (S)-4-(4-hydrazmobenzyl)-1,3-oxazolidin-2-one prepared by diazotation 1.75 kg of the amine (I) and reduction in accordance with the above mentioned scheme is heated up to ca. 90C. 1.75 kg of <strong>[1116-77-4]4,4-diethoxy-N,N-dimethylbutylamine</strong> of formula II is weighed. The weighed acetal (II) is added to the reaction mixture, which is then brought to moderate reflux at ca. 980C and left to react being stirred under a reflux condenser for 2.5 hours. After 2.5 hours from the start of the reflux the heating of the mixture is switched off and the reaction mixture is cooled to the laboratory temperature.
 

Historical Records

Technical Information

Categories