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Chemical Structure| 182876-24-0 Chemical Structure| 182876-24-0

Structure of 182876-24-0

Chemical Structure| 182876-24-0

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Product Details of [ 182876-24-0 ]

CAS No. :182876-24-0
Formula : C11H18O
M.W : 166.26
SMILES Code : OCC1CC2(C1)CC1(CCC1)C2
MDL No. :MFCD29046323

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Application In Synthesis of [ 182876-24-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 182876-24-0 ]

[ 182876-24-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 28114-87-6 ]
  • [ 182876-24-0 ]
  • dispiro[3.1.3.1]decan-2-ylmethyl spiro[3.3]heptane-2-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
56.3% With toluene-4-sulfonic acid; In tetrahydrofuran; benzene; for 4.0h;Dean-Stark; Heating; 225 mg (1.6 mmol) of spiro [3,3] heptane-2-carboxylic acid and 500 mg (1.9 mmol) ofIsopyro [3,1,3,1] decan-2-ylmethanolAnd314 mg (1.6 mmol) of para-toluenesulfonic acid was dissolved in 7 ml of benzene solution and 3 ml of tetrahydrofuran solution, followed by stirring at 80 C with a Dean-Stark trap.After 4 hours, the organic material was extracted with 15 ml of distilled water and 15 ml of ethyl ether. The organic extracts were dried over anhydrous magnesium sulfate, and the solvent was concentrated under reduced pressure. 254 mg (0.9 mmol, spiro [3,3] heptane-2-carboxylic acid : 56.3%) of the compound represented by the formula (11) was obtained.
 

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