Home Cart Sign in  
Chemical Structure| 17432-37-0 Chemical Structure| 17432-37-0

Structure of 17432-37-0

Chemical Structure| 17432-37-0

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 17432-37-0 ]

CAS No. :17432-37-0
Formula : C11H14O
M.W : 162.23
SMILES Code : O=CC1=C(C)C(C)=CC(C)=C1C
MDL No. :MFCD02249226

Safety of [ 17432-37-0 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 17432-37-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 17432-37-0 ]

[ 17432-37-0 ] Synthesis Path-Downstream   1~3

  • 2
  • [ 1967-89-1 ]
  • [ 33513-42-7 ]
  • [ 7072-01-7 ]
  • [ 17432-37-0 ]
  • 3
  • [ 1646-53-3 ]
  • [ 33513-42-7 ]
  • [ 17432-37-0 ]
YieldReaction ConditionsOperation in experiment
52% To a stirred solution of 3-Bromo-1,2,4,5-tetramethylbenzene, 1 (5 gm, 23.5 mmol) in anhydrous THF (60 mL) at -78 C, n-BuLi (10 mL, 24.6 mml, 2M in hexane) solution was added dropwise. The reaction mixture was stirred at the same temperature for further 1 hr. Anhydrous dimethyl formamide (3.6 mL, 47.0 mmol) was added dropwise to the mixture at -78 C and stirred for 1 hr. The reaction mixture slowly warmed to 0 C and quenched with saturated aqueous solution of NH4Cl. The aqueous layer was extracted with ethyl acetate (3*100 mL) then organic layer was washed with saturated brine solution. The combined organic layer was dried over anhydrous Na2SO4, filtered, concentrated under reduced pressure. The crude reaction mixture was purified on silica gel column chromatography to obtainpure aldehyde (2.0 gm, 52%) and the analytical data was matched with literature reported data.
 

Historical Records

Technical Information

Categories