17243-13-9|5-(Chlorosulfonyl)-2-hydroxybenzoic acid| Ambeed

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Quality Control of [ 17243-13-9 ] Purity: 95% SDS Specification

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Product Details of [ 17243-13-9 ]

CAS No. :	17243-13-9
Formula :	C₇H₅ClO₅S
M.W :	236.63
SMILES Code :	OC(=O)C1=C(O)C=CC(=C1)S(Cl)(=O)=O
MDL No. :	MFCD00052974

Safety of [ 17243-13-9 ]

GHS Pictogram:
Signal Word:	Danger
Hazard Statements:	H314
Precautionary Statements:	P280-P305+P351+P338-P310
Class:	8
UN#:	3261
Packing Group:	Ⅲ

Application In Synthesis of [ 17243-13-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 17243-13-9 ]

[ 17243-13-9 ] Synthesis Path-Downstream 1~35

1
[ 54-21-7 ]
[ 17243-13-9 ]

References: [1]Zhurnal Obshchei Khimii,1950,vol. 20,p. 1818,1823; engl. Ausg. S. 1883, 1888.

2
[ 134-32-7 ]
[ 17243-13-9 ]
2-hydroxy-5-[1]naphthylsulfamoyl-benzoic acid [ No CAS ]

References: [1]Yakugaku Zasshi/Journal of the Pharmaceutical Society of Japan,1951,vol. 71,p. 969,971.
Chem.Abstr.,1952,p. 8043.

3
[ 1709-59-7 ]
[ 17243-13-9 ]
5-(4-dimethylsulfamoyl-phenylsulfamoyl)-2-hydroxy-benzoic acid [ No CAS ]

References: [1]Patent: US2256274,1939, .

4
[ 118-46-7 ]
[ 17243-13-9 ]
2-hydroxy-5-(7-hydroxy-[1]naphthylsulfamoyl)-benzoic acid [ No CAS ]

References: [1]Patent: DE276331, .
Fortschr. Teerfarbenfabr. Verw. Industriezweige,vol. 12,p. 173.

5
[ 128-95-0 ]
[ 17243-13-9 ]
6,6'-dihydroxy-3,3'-(9,10-dioxo-9,10-dihydro-anthracene-1,4-diyldisulfamoyl)-di-benzoic acid [ No CAS ]

References: [1]Patent: DE405643, .
Fortschr. Teerfarbenfabr. Verw. Industriezweige,vol. 14,p. 858.

6
[ 145-49-3 ]
[ 17243-13-9 ]
1,5-bis-(3-carboxy-4-hydroxy-benzenesulfonylamino)-4,8-dihydroxy-anthraquinone [ No CAS ]

References: [1]Patent: DE405643, .
Fortschr. Teerfarbenfabr. Verw. Industriezweige,vol. 14,p. 858.

7
[ 1709-52-0 ]
[ 17243-13-9 ]
2-hydroxy-5-(4-methylsulfamoyl-phenylsulfamoyl)-benzoic acid [ No CAS ]

References: [1]Patent: US2256274,1939, .

8
[ 93-36-7 ]
[ 17243-13-9 ]
2-hydroxy-5-(7-hydroxy-[2]naphthylsulfamoyl)-benzoic acid [ No CAS ]

References: [1]Patent: DE276331, .
Fortschr. Teerfarbenfabr. Verw. Industriezweige,vol. 12,p. 173.

9
[ 50-01-1 ]
[ 17243-13-9 ]
5-carbamimidoylsulfamoyl-2-hydroxy-benzoic acid [ No CAS ]

References: [1]Arkiv foer Kemi,1947,vol. 34 A,p. 6.

10
[ 17243-13-9 ]
[ 118-92-3 ]
<i>N</i>-(3-carboxy-4-hydroxy-benzenesulfonyl)-anthranilic acid [ No CAS ]

References: [1]Yakugaku Zasshi/Journal of the Pharmaceutical Society of Japan,1951,vol. 71,p. 969,971.
Chem.Abstr.,1952,p. 8043.

11
[ 17243-13-9 ]
[ 63-74-1 ]
[ 126884-27-3 ]

References: [1]Anales de la Real Sociedad Espanola de Fisica y Quimica,1947,vol. 43,p. 623,626.

12
[ 127-09-3 ]
[ 17243-13-9 ]
[ 62-53-3 ]
[ 62547-03-9 ]

References: [1]Patent: DE276331, .
Fortschr. Teerfarbenfabr. Verw. Industriezweige,vol. 12,p. 173.

13
[ 17243-13-9 ]
[ 156-43-4 ]
[ 92851-92-8 ]

References: [1]Patent: DE276331, .
Fortschr. Teerfarbenfabr. Verw. Industriezweige,vol. 12,p. 173.

14
[ 17243-13-9 ]
[ 99-09-2 ]
[ 62547-13-1 ]

References: [1]Patent: DE276331, .
Fortschr. Teerfarbenfabr. Verw. Industriezweige,vol. 12,p. 173.

15
[ 17243-13-9 ]
[ 92-87-5 ]
4,4'-bis-(3-carboxy-4-hydroxy-benzenesulfonylamino)-biphenyl [ No CAS ]

References: [1]Journal of Organic Chemistry,1954,vol. 19,p. 56,58.

16
[ 17243-13-9 ]
[ 122-80-5 ]
5-(4-acetylamino-phenylsulfamoyl)-2-hydroxy-benzoic acid [ No CAS ]

References: [1]Yakugaku Zasshi/Journal of the Pharmaceutical Society of Japan,1951,vol. 71,p. 969,971.
Chem.Abstr.,1952,p. 8043.

17
[ 17243-13-9 ]
[ 121-57-3 ]
2-hydroxy-5-(4-sulfo-phenylsulfamoyl)-benzoic acid [ No CAS ]

References: [1]Yakugaku Zasshi/Journal of the Pharmaceutical Society of Japan,1951,vol. 71,p. 969,971.
Chem.Abstr.,1952,p. 8043.

18
[ 17243-13-9 ]
[ 58765-12-1 ]

References: [1]Diss. <E.T.H. Zuerich 1929> S. 97,.

19
[ 17243-13-9 ]
[ 24619-05-4 ]

References: [1]Inorganica Chimica Acta,2011,vol. 368,p. 231 - 236.
[2]Journal of the Chemical Society,1922,vol. 121,p. 2558.
[3]Yakugaku Zasshi/Journal of the Pharmaceutical Society of Japan,1957,vol. 77,p. 963.
Chem.Abstr.,1958,p. 2792.

20
[ 17243-13-9 ]
[ 19479-88-0 ]

References: [1]Journal of Medicinal Chemistry,1986,vol. 29,p. 25 - 29.
[2]Patent: US1766946,1925, .

21
[ 97-05-2 ]
[ 17243-13-9 ]

References: [1]Journal of the Chemical Society,1922,vol. 121,p. 2558.
[2]Polyhedron,2010,vol. 29,p. 226 - 231.
[3]Journal of Fluorescence,2011,vol. 21,p. 653 - 662.

22
[ 69-72-7 ]
[ 17243-13-9 ]

Yield	Reaction Conditions	Operation in experiment
60%	With chlorosulfonic acid;	EXAMPLE 1 Synthesis of 5-chlorosulfonylsalicylic acid To 125 ml of chlorosulfonic acid in a round bottom flask, cooled with an ice bath, was slowly added 25 g. of salicylic acid with constant stirring. After all the salicylic acid was dissolved the cool mixture was heated in an oil bath, at 75 C. under constant stirring, for about 1 hour. The heated mixture was then carefully poured onto about 500 g. of crushed ice forming a white solid. The white solid was collected in a Buchner funnel and was recrystallized from CH2 Cl2 to provide a 60% yield of a product having a melting point of 170-172 C. and identified as 5-chlorosulfonylsalicylic acid.
	With chlorosulfonic acid; at 0 - 70℃; for 3h;	EXAMPLE A5; 2-Cyclopentyloxy-5-methylsulfamoyl-benzoic acid; (a) 5-Chlorosulfonyl-2-hydroxy-benzoic acid; To 3.26 mol chlorosulfonic acid at 0 C. was added 652 mmol salicylic acid in small portions, and the mixture was then allowed to stir at RT for 1 h, then at 50 C. for 1 h, and finally at 70 C. for 1 h. The mixture was then added dropwise to 1000 ml ice-water with stirring and stirring continued for an additional 30 min. The ensuing white crystals were collected by filtration, washed three times with water, and then dried in vacuo at 45 C. for 16 h to yield the title compound.
	With chlorosulfonic acid; at 0 - 70℃; for 3h;	(a) 5-Chlorosulfonvl-2-hvdroxv-benzoic acid; To 3.26 mol chlorosulfonic acid at 0 0C was added 652 mmol salicylic acid in small portions and the mixture was then allowed to stir at RT for 1 h, then at 50 0C for 1 h, and finally at 70 0C for 1 h. The mixture was then added dropwise to 1000 ml ice-water with stirring and stirring continued for an additional 30 min. The ensuing white crystals were collected by filtration, washed three times with water, and then dried in vacuo at 45 0C for 16 h to yield the title compound. MS (m/e): 236.8 ([(37Cl)M-H]", 33%), 235.0 ([{37C1}M- H]", 100%)

	With chlorosulfonic acid; at 20 - 70℃; for 3h;	EXAMPLE B13 2-Methoxy-5-methylsulfamoyl-benzoic acid (a) 5-Chlorosulfonyl-2-hydroxy-benzoic acid; To 3.26 mol chlorosulfonic acid at 0 C. was added 652 mmol salicylic acid in small portions and the mixture was then allowed to stir at RT for 1 h, then at 50 C. for 1 h, and finally at 70 C. for 1 h. The mixture was then added dropwise to 1000 ml ice-water with stirring and stirring continued for an additional 30 min. The ensuing white crystals were collected by filtration, washed three times with water, and then dried in vacuo at 45 C. for 16 h to yield the title compound. MS (m/e): 236.8 ([{37Cl}M-H]-, 33%), 235.0 ([{37Cl}M-H]-, 100%)
	With chlorosulfonic acid; thionyl chloride; at 0 - 25℃; for 15.9167h;	Example 1Preparation of 2- hydroxy-5-(4 methyl)-l-piperazinyl sulphonyl) benzoic acid Step-1: Preparation of 5-Chlorosulfonyl-2-hydroxy benzoic acidTo the chilled chlorosulfonic acid (1012 g), salicylic acid (200 g) was added at 0-50C over a period of 1 hour 40 min. The temperature of the reaction mixture was maintained at 20-250C for 2 hrs. Then thionyl chloride (172.4 g) was added over a period of 15 min and maintained for 12 hrs. The product formed was poured onto ice and maintained for lhr. The product was filtered and washed with DM water to get 5-Chlorosulfonyl-2- hydroxy benzoic acid.

References: [1]Phosphorus, Sulfur and Silicon and the Related Elements,1991,vol. 57,p. 75 - 81.
[2]Journal of Medicinal Chemistry,1986,vol. 29,p. 25 - 29.
[3]Phosphorus and Sulfur and the Related Elements,1981,vol. 10,p. 323 - 332.
[4]Patent: US4939132,1990,A .
[5]Journal of the Chemical Society,1922,vol. 121,p. 2558.
[6]Patent: US2006/160788,2006,A1 .Location in patent: Page/Page column 11.
[7]Patent: WO2006/72436,2006,A1 .Location in patent: Page/Page column 31.
[8]Patent: US2006/178381,2006,A1 .Location in patent: Page/Page column 67.
[9]Patent: WO2007/141805,2007,A2 .Location in patent: Page/Page column 6; 11.
[10]Patent: DE264786, .
Fortschr. Teerfarbenfabr. Verw. Industriezweige,vol. 11,p. 216.

23
[ 17243-13-9 ]
[ 83-31-8 ]
5-(2,2-dioxo-2λ⁶-naphth[1,8-<i>cd</i>][1,2]oxathiol-6-sulfonyl)-2-hydroxy-benzoic acid [ No CAS ]

References: [1]Helvetica Chimica Acta,1947,vol. 30,p. 1650,1660.
[2]Helvetica Chimica Acta,1947,vol. 30,p. 1650,1660.

24
[ 110-91-8 ]
[ 17243-13-9 ]
[ 91134-85-9 ]

References: [1]Journal of general chemistry of the USSR,1963,vol. 33,p. 388 - 390.
Zhurnal Obshchei Khimii,1963,vol. 33,p. 394 - 396.

25
[ 49739-65-3 ]
[ 17243-13-9 ]
2-Hydroxy-5-(9-methoxy-7-oxo-7H-furo[3,2-g]chromen-4-ylsulfamoyl)-benzoic acid [ No CAS ]

References: [1]Journal of the Indian Chemical Society,1988,vol. 65,p. 422 - 426.

26
[ 108-24-7 ]
[ 17243-13-9 ]
2-acetoxy-5-chlorosulfonylbenzoic acid [ No CAS ]

References: [1]Phosphorus and Sulfur and the Related Elements,1980,vol. 9,p. 155 - 164.

27
[ 704-56-3 ]
[ 17243-13-9 ]
2-Hydroxy-5-(5-pyridin-4-yl-[1,3,4]oxadiazol-2-ylsulfamoyl)-benzoic acid [ No CAS ]

References: [1]Journal of the Indian Chemical Society,1988,vol. 65,p. 357 - 361.

28
[ 17243-13-9 ]
[ 108-91-8 ]
2-hydroxy-5-N-(cyclohexyl)sulfonamidobenzoic acid [ No CAS ]

References: [1]Phosphorus and Sulfur and the Related Elements,1980,vol. 9,p. 155 - 164.

29
[ 17243-13-9 ]
[ 62-53-3 ]
[ 62547-03-9 ]

References: [1]Phosphorus and Sulfur and the Related Elements,1980,vol. 9,p. 155 - 164.

30
[ 17243-13-9 ]
[ 5059-82-5 ]

References: [1]Phosphorus and Sulfur and the Related Elements,1981,vol. 10,p. 323 - 332.

31
[ 17243-13-9 ]
[ 17645-94-2 ]

References: [1]Phosphorus, Sulfur and Silicon and the Related Elements,1991,vol. 57,p. 75 - 81.

32
[ 50-78-2 ]
[ 17243-13-9 ]

References: [1]Phosphorus and Sulfur and the Related Elements,1980,vol. 9,p. 155 - 164.

33
[ 135251-12-6 ]
[ 17243-13-9 ]

References: [1]Archiv der Pharmazie,1995,vol. 328,p. 283 - 285.

34
[ 17243-13-9 ]
[ 211361-50-1 ]
2-Hydroxy-5-{5-[1-(4-isobutyl-phenyl)-ethyl]-[1,3,4]oxadiazol-2-ylsulfamoyl}-benzoic acid [ No CAS ]

References: [1]Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry,1996,vol. 35,p. 1062 - 1066.

35
[ 17243-13-9 ]
2-amino-4-[2-(p-chlorobenzenesulphonamido)phenyl]thiazole [ No CAS ]
5-{4-[2-(4-chloro-benzenesulfonylamino)-phenyl]-thiazol-2-ylsulfamoyl}-2-hydroxy-benzoic acid [ No CAS ]

References: [1]Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry,1999,vol. 38,p. 696 - 700.

Historical Records

Technical Information

• Alkyl Halide Occurrence • Arndt-Eistert Homologation • General Reactivity • Grignard Reaction • Hiyama Cross-Coupling Reaction • Hunsdiecker-Borodin Reaction • Kinetics of Alkyl Halides • Kumada Cross-Coupling Reaction • Passerini Reaction • Preparation of Amines • Preparation of Carboxylic Acids • Reactions of Alkyl Halides with Reducing Metals • Reactions of Amines • Reactions of Benzene and Substituted Benzenes • Reactions of Carboxylic Acids • Schmidt Reaction • Specialized Acylation Reagents-Ketenes • Stille Coupling • Substitution and Elimination Reactions of Alkyl Halides • Suzuki Coupling • Ugi Reaction

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H317	May cause an allergic skin reaction
H318	Causes serious eye damage
H319	Causes serious eye irritation
H320	Causes eye irritation
H330	Fatal if inhaled
H331	Toxic if inhaled
H332	Harmful if inhaled
H333	May be harmful if inhaled
H334	May cause allergy or asthma symptoms or breathing difficulties if inhaled
H335	May cause respiratory irritation
H336	May cause drowsiness or dizziness
H340	May cause genetic defects
H341	Suspected of causing genetic defects
H350	May cause cancer
H351	Suspected of causing cancer
H360	May damage fertility or the unborn child
H361	Suspected of damaging fertility or the unborn child
H361d	Suspected of damaging the unborn child
H362	May cause harm to breast-fed children
H370	Causes damage to organs
H371	May cause damage to organs
H372	Causes damage to organs through prolonged or repeated exposure
H373	May cause damage to organs through prolonged or repeated exposure
Environmental hazards
Code	Phrase
H400	Very toxic to aquatic life
H401	Toxic to aquatic life
H402	Harmful to aquatic life
H410	Very toxic to aquatic life with long-lasting effects
H411	Toxic to aquatic life with long-lasting effects
H412	Harmful to aquatic life with long-lasting effects
H413	May cause long-lasting harmful effects to aquatic life
H420	Harms public health and the environment by destroying ozone in the upper atmosphere

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CAS No.: 17243-13-9

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CAS No.: 17243-13-9

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[ 17243-13-9 ] Synthesis Path-Downstream 1~35

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