Home Cart Sign in  
HazMat Fee +

There will be a HazMat fee per item when shipping a dangerous goods. The HazMat fee will be charged to your UPS/DHL/FedEx collect account or added to the invoice unless the package is shipped via Ground service. Ship by air in Excepted Quantity (each bottle), which is up to 1g/1mL for class 6.1 packing group I or II, and up to 25g/25ml for all other HazMat items.

Type HazMat fee for 500 gram (Estimated)
Excepted Quantity USD 0.00
Limited Quantity USD 15-60
Inaccessible (Haz class 6.1), Domestic USD 80+
Inaccessible (Haz class 6.1), International USD 150+
Accessible (Haz class 3, 4, 5 or 8), Domestic USD 100+
Accessible (Haz class 3, 4, 5 or 8), International USD 200+
Chemical Structure| 17231-95-7 Chemical Structure| 17231-95-7

Structure of 17231-95-7

Chemical Structure| 17231-95-7

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Product Citations

Markwitz, Martyna ; Labrzycki, Klaudiusz ; Azcune, Laura ; Landa, Aitor ; Kucinski, Krzysztof ;

Abstract: A metal-free dehydrative thioetherification method has been reported, enabling the conversion of various alcs. and thiols into thioethers. By employing triflic acid as a catalyst or utilizing a recyclable NAFION superacid catalyst, these methods significantly improve the efficiency and practicality of sulfide preparation

Purchased from AmBeed: ; ; ; ;

Alternative Products

Product Details of [ 17231-95-7 ]

CAS No. :17231-95-7
Formula : C6H4Cl2S
M.W : 179.07
SMILES Code : SC1=CC=CC(Cl)=C1Cl
MDL No. :MFCD00041420

Safety of [ 17231-95-7 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302-H318
Precautionary Statements:P280-P305+P351+P338
Class:8
UN#:1759
Packing Group:

Application In Synthesis of [ 17231-95-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 17231-95-7 ]

[ 17231-95-7 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 3034-57-9 ]
  • [ 17231-95-7 ]
  • [ 17119-36-7 ]
  • 2
  • [ 17231-95-7 ]
  • [ 2401-21-0 ]
  • [ 1046803-83-1 ]
YieldReaction ConditionsOperation in experiment
68% With tetrakis(triphenylphosphine) palladium(0); caesium carbonate; In toluene; at 110℃; for 16h;Inert atmosphere; General procedure: The studied solid TCDPSs were synthesized by ourselves. The general synthetic route is [21]: When it comes to the 4 title compounds, the specific reactantsand yields are shown in Table 1. The following steps were adopted. 1 mmol of chloro thiophenol was dissolved in 10 ml of toluene. Next, 1 mmol of chloro iodobenzene and 2.5 mmol of cesium carbonate, together with 0.1 mmol of tetrakis (triphenylphosphine) palladium (Pd(PPh3)4, used as catalyst) were added into the mixture and the solution was heated to about 110 .C for 16 h under nitrogen. After cooling to room temperature, the solution was diluted with 100 ml of water and extracted 3 times with 20 ml of petroleum ether. The extract was dried with anhydrous magnesium sulfate, filtered and concentrated. The crude product obtained was further eluted with petroleum ether and then purified by silica gel column chromatography (300.400 mesh). Thus, the target products of high purity can be used for the determination of spectral properties. The IR spectra of the title compounds diluted in the KBr pellets were measured on a Nexus 470 FTIR spectrophotometer in the range of 400.4000 cm.1 at room temperature. The 1H NMR and 13C NMR measurements were carried out using a Bruker Avance NMR spectrometer operating at 400 MHz at room temperature with TMS as an internal standard in CDCl3.
 

Historical Records