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Chemical Structure| 169045-13-0 Chemical Structure| 169045-13-0

Structure of 169045-13-0

Chemical Structure| 169045-13-0

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Product Details of [ 169045-13-0 ]

CAS No. :169045-13-0
Formula : C9H10N2O
M.W : 162.19
SMILES Code : N#CC1=CC(CN)=CC=C1OC
MDL No. :MFCD18394240

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Application In Synthesis of [ 169045-13-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 169045-13-0 ]

[ 169045-13-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 169045-13-0 ]
  • [ 178308-61-7 ]
  • [ 240400-76-4 ]
YieldReaction ConditionsOperation in experiment
1,8-diazabicyclo[5.4.0]undec-7-ene; In 1-methyl-pyrrolidin-2-one; 1,4-Dichlorophthalazine-6-carbonitrile and 3-cyano-4-methoxybenzylamine were stirred at room temperature in 1-methyl-2-pyrrolidinone in the presence of DBU, whereby 1-chloro-4-[(3-cyano-4-methoxybenzyl)amino]-6-phthalazine carbonitrile was obtained as a less polar product. 1H-NMR (400 MHz, DMSO-d6) δ; 3.87 (3H, s), 4.70 (2H, d, J=5.6 Hz), 7.20 (1H, d, J=8.4 Hz), 7.70 (1H, dd, J=2.4, 8.4 Hz), 7.75 (1H, d, J=2.4 Hz), 8.19 (1H, d, J=8.4 Hz), 8.34 (1H, dd, J=1.2, 8.4 Hz), 8.48 (1H, t, J=5.6 Hz), 8.97 (1H, s).
 

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